ISSN: 0256-1115 (print version) ISSN: 1975-7220 (electronic version)
Copyright © 2024 KICHE. All rights reserved

Articles & Issues

Language
English
Conflict of Interest
In relation to this article, we declare that there is no conflict of interest.
Publication history
Received March 28, 2003
Accepted May 21, 2003
articles This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
Copyright © KIChE. All rights reserved.

All issues

Maximization of Total Surface Area of Pt-SnO2/Al2O3 Catalyst by the Taguchi Method

Department of Chemical Engineering, Bogazici University, Bebek, 80815 Istanbul, Turkey 1Department of Chemical Engineering, Kocaeli University, Veziroglu Campus, 41040 Kocaeli, Turkey
Korean Journal of Chemical Engineering, September 2003, 20(5), 840-843(4), 10.1007/BF02697285
downloadDownload PDF

Abstract

The maximization of the total surface area of Pt-SnO2/Al2O3 catalyst was studied by using the Taguchi method of experimental design. The catalysts were prepared by sol-gel method. The effects of HNO3, H2O and aluminum nitrate concentrations and the stirring rate on the total surface area were studied at three levels of each. L9 orthogonal array leading nine experiments was used in the experimental design. The parameter levels that give maximum total surface area were determined and experimentally verified. In the range of conditions studied it was found that, medium levels of HNO3 and H2O concentration and lower levels of aluminum nitrate concentration and stirring rate maximize the total surface area.

References

Cho IH, Park SB, Cho SJ, Ryoo R, J. Catal., 173(2), 295 (1998) 
Dawson EA, Barnes PA, Appl. Catal. A: Gen., 90, 217 (1992) 
Ko EI, "Sol-Gel Process," Preparation of Solid Catalysts, G. Ertl, H. Knozinger, J. Weitkamp, eds. Wiley-VCH, Weinheim (1999)
Montgomery DC, "Design and Analysis of Experiments," 5th ed., John Wiley & Son, New York (2001)
Phadke MS, "Quality Engineering Using Robust Design," Prentice-Hall, Englewood Cliffs (1989)
Rezgui S, Jentoft R, Gates BC, J. Catal., 163(2), 496 (1996) 
Schmidt F, Appl. Catal. A: Gen., 221(1-2), 15 (2001) 
Sheth A, Trembath K, J. Mater. Process. Tech., 123, 167 (2002) 
Taguchi G, "Introduction to Quality Engineering," Asian Productivity Organization, (Distributed by American Suppliers Institute, Inc., Dearborn, MI) (1986)
Trimm DL, Onsan ZI, Catal. Rev.-Sci. Eng., 43(1-2), 31 (2001) 
Wan HP, Chyang CS, Korean J. Chem. Eng., 16(5), 654 (1999)
Yang DW, Hung KM, Hsieh CS, Mater. Sci. Eng. A, 333, 123 (2002) 

The Korean Institute of Chemical Engineers. F5, 119, Anam-ro, Seongbuk-gu, 233 Spring Street Seoul 02856, South Korea.
TEL. No. +82-2-458-3078FAX No. +82-507-804-0669E-mail : kiche@kiche.or.kr

Copyright (C) KICHE.all rights reserved.

- Korean Journal of Chemical Engineering 상단으로