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Received November 14, 2006
Accepted August 5, 2007
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Solubility of 4-(3,4-dichlorophenyl)-1-tetralone in eleven alcohols with the temperature range from 283K to 323K
College of Chemical Engineering, Beijing University of Chemical Technology, Beijing 100029, China
lantianxia2005@sohu.com
Korean Journal of Chemical Engineering, May 2008, 25(3), 558-561(4), 10.1007/s11814-008-0094-2
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Abstract
The solubility of 4-(3,4-dichlorophenyl)-1-tetralone in eleven alcohols (methanol, ethanol, 1-propanol, 1-butanol, 1-pentanol, 1-hexanol, 2-propanol, 2-butanol, 2-pentanol, 1,2-propanediol, 1,3-propanediol) was measured by using a laser technique with a temperature range from 283 K to 323 K, and at atmospheric pressure. For mono n-alcohols, the solubility is the lowest in methanol, increasing with the carbon chain of the alcohols. The results were correlated with a semi-empirical equation. The experimental solubility and correlation equation in this work can be used as essential data and models in the purification process of 4-(3,4-dichlorophenyl)-1-tetralone.
References
Krisztina V, Tamas F, Janos F, Iren F, Sandor L, Organic Process & Development, 6, 82 (2002)
Geraldine PT, David MP, Juan CC, Organic Process & Development, 8, 385 (2004)
Jaesook Y, Stephen LB, J. Org. Chem., 65, 767 (2000)
Heffter GT, Tomkins RPT, John Wiley, Chichester, 260 (2003)
Kim KS, Demberelnyamba D, Shin BK, Yeon SH, Choi S, Cha JH, Lee H, Lee CS, Shim JJ, Korean J. Chem. Eng., 23(1), 113 (2006)
Wang S, Chen D, Korean J. Chem. Eng., 23(6), 1034 (2006)
Ren GB, Wang JK, Yin QX, Zhang MJ, J. Chem. Eng. Data, 49, 1671 (2004)
Wang S, Wang JK, Yin QX, Wang YL, Chinese Optics Letters, 3, 149 (2005)
Wang S, Wang JK, Yin QX, Ind. Eng. Chem. Res., 44(10), 3783 (2005)
Li XN, Yin QX, Chen W, Wang JK, J. Chem. Eng. Data, 51, 127 (2006)
Hao HX, Wang JK, Wang YL, J. Chem. Eng. Data, 49, 1697 (2004)
Li DQ, Liu DZ, Wang FA, J. Chem. Eng. Data, 46, 234 (2001)
Geraldine PT, David MP, Juan CC, Organic Process & Development, 8, 385 (2004)
Jaesook Y, Stephen LB, J. Org. Chem., 65, 767 (2000)
Heffter GT, Tomkins RPT, John Wiley, Chichester, 260 (2003)
Kim KS, Demberelnyamba D, Shin BK, Yeon SH, Choi S, Cha JH, Lee H, Lee CS, Shim JJ, Korean J. Chem. Eng., 23(1), 113 (2006)
Wang S, Chen D, Korean J. Chem. Eng., 23(6), 1034 (2006)
Ren GB, Wang JK, Yin QX, Zhang MJ, J. Chem. Eng. Data, 49, 1671 (2004)
Wang S, Wang JK, Yin QX, Wang YL, Chinese Optics Letters, 3, 149 (2005)
Wang S, Wang JK, Yin QX, Ind. Eng. Chem. Res., 44(10), 3783 (2005)
Li XN, Yin QX, Chen W, Wang JK, J. Chem. Eng. Data, 51, 127 (2006)
Hao HX, Wang JK, Wang YL, J. Chem. Eng. Data, 49, 1697 (2004)
Li DQ, Liu DZ, Wang FA, J. Chem. Eng. Data, 46, 234 (2001)
