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Received September 28, 2009
Accepted December 16, 2009
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Preparation and characteristics of nano-B4C/PVA particles and ultra high molecular weight polyethylene composites
Nuclear Materials Research Division, Korea Atomic Energy Research Institute, 1045 Daedukdaero, Daejeon 305-353, Korea
kimj@kaeri.re.kr
Korean Journal of Chemical Engineering, July 2010, 27(4), 1338-1342(5), 10.1007/s11814-010-0200-0
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Abstract
In-situ mechanical process for preparation of the polyvinyl alcohol (PVA) coated nano-B4C powder was investigated by using a high-energy ball mill. The produced PVA coat on the surface of nano-B4C particles was observed by x-ray diffraction (XRD) and confirmed by TEM images. The average particle size of the produced nano-B4C/PVA particles was in the range of several tens to hundreds of nanometers depending on the milling conditions. The polymer composites were fabricated by hot pressing ultra high molecular weight polyethylene (UHMWPE) powder_x000D_
mixed with nano-B4C/PAV and micro-B4C powders, respectively. Nano-B4C/PVA dispersed UHMWPE shows slightly lower crystallinity and stiffness than micro-B4C dispersed UHMWPE based on differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA) evaluations.
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References
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Tucker JD, Lear PL, Atkinson GS, Lee S, Lee SJ, Korean J. Chem. Eng., 17(5), 506 (2000)
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Venkataraman KS, Narayanan KS, Powder Technol., 96(1), 190 (1998)
Magini M, Iasonna A, Padella F, Scripta Mater., 34(1), 13 (1996)
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Castillo JM, Lapasin R, Grassi M, Ind. Eng. Chem. Res., 42(9), 2015 (2003)
Kong Y, Hay JN, Polymer., 42, 3873 (2002)
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