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Received December 21, 2010
Accepted February 20, 2011
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Effects of sodium dodecyl benzenesulfonic acid (SDBS) on the morphology and the crystal phase of CaCO3
Dae Ju Hwang1 2
Kye Hong Cho1
Moon Kwan Choi1
Young Hwan Yu1
Seung Kwan Lee1
Ji Whwan Ahn3
Gwang Il Lim4
Choon Han4†
Jong Dae Lee2
1Korea Institute of Limestone and Advanced Materials, 63, Wooduk-ri, Maepo-up, Danyang-gun, Chungbuk 395-903, Korea 2Department of Chemical Engineering, Chungbuk National University, 410 Sungong-ro, Heungduk-gu, Chung-ju, Chungbuk 361-763, Korea 3Mineral Processing Department, Mineral Resources Research Division, Korea Institute of Geoscience and Mineral Resources, 92-Science-ro, Yuseong-gu, Daejeon 305-350, Korea 4Department of Chemical Engineering, Kwangwoon University, 447-1 Wolgye-dong, Nowon-gu, Seoul 139-701, Korea
chan@kw.ac.kr
Korean Journal of Chemical Engineering, September 2011, 28(9), 1927-1935(9), 10.1007/s11814-011-0044-2
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Abstract
The effects of anionic surfactant on the morphology and crystallization of calcium carbonate precipitated from CaCl2 and Na2CO3 were investigated. Although reaction temperature did not have an effect on the morphology of calcium carbonate, it did have an effect on the cluster size. The cluster size became bigger with high reaction temperature. With the addition of sodium dodecyl benzenesulfonic acid (SDBS), the morphology of precipitated calcium carbonate changed from cubic to porous spheres with over 98% of the crystal phase transformed from calcite to vaterite. The analysis of precipitates formed by the reaction of CaCl2 solution (from limestone (CaO 50% content)) and Na2CO3 found that the morphology of precipitated calcium carbonate changed from cubic to spherical, and the crystal phase changed from calcite to over 94% vaterite with the addition of sodium dodecyl benzenesulfonic acid. These vaterite structures were solid spheres rather than hollow ones.
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Yu J, Lei M, Cheng B, J. Solid State Chem., 177, 681 (2004)
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Petrov AI, Volodkin DV, Sukhorukov GB, Biotechnol. Prog., 21(3), 918 (2005)
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Gehrke N, COlfen H, Pinna N, Cryst. Growth Des., 1317, 5 (2005)
Li M, Schnablegger H, Mann S, Nature., 393, 402 (1999)
