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Received December 5, 2013
Accepted April 8, 2014
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Ion imprinted activated carbon solid-phase extraction coupled to flame atomic absorption spectrometry for selective determination of lead ions in environmental samples
Department of Environmental Engineering, Faculty of Environmental and Energy, Science Research Branch, Islamic Azad University, Tehran, Iran 1Department of Chemistry, Central Tehran Branch, Islamic Azad University, Tehran, Iran 2Department of Chemistry, Varamin (Pishva) Branch, Islamic Azad University, Varamin, Iran
h.ahmadpanahi@iauctb.ac.ir
Korean Journal of Chemical Engineering, October 2014, 31(10), 1818-1823(6), 10.1007/s11814-014-0104-5
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Abstract
A simple lead ion imprinted sorbent was synthesized by coupling activated carbon with a known metal chelating compound, iminodiacetic acid. The ion imprinted sorbent has been characterized using Fourier transform infrared spectroscopy, elemental analysis and thermogravimetric analysis and subjected for the extraction and determination of trace Pb(II) in environmental water samples. The optimum pH value for sorption of the lead ion was 6.5. The sorption capacity of lead imprinted sorbent was 42.2 mg g^(-1). The chelating imprinted sorbent can be reused for five cycles of sorption-desorption without any significant change in sorption capacity. Compared with non-imprinted polymer particles, the lead ion imprinted sorbent showed high adsorption capacity, significant selectivity, good site accessibility for Pb(II). The equilibrium adsorption data of Pb(II) by modified resin were analyzed by Langmuir, Freundlich, Temkin and Redlich-Peterson models.
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Kagaya S, Araki Y, Hasegawa K, Fresenius J. Anal. Chem., 366, 842 (2000)
Kaqava S, Malek ZA, Araki Y, Haseqawa K, Anal. Sci., 18, 923 (2002)
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Elci L, Arslan Z, Tyson JF, Spectrochim. Acta Part B, 55, 1109 (2000)
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Han DM, Fang GZ, Yan XP, J. Chromatogr. A, 1100, 131 (2005)
Jiang X, Zhao C, Jiang N, Zhang H, Liu M, Food Chem., 108, 1061 (2008)
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Xie F, Lin X, Wu X, Xie Z, Talanta, 74, 836 (2008)
Vinicius L, Gurgel A, Pereira de Freitas R, Frederic Gil L, Carbohydr. Polym., 74, 922 (2008)
Chen D, Hu B, Huang C, Talanta, 78, 491 (2009)
Filiz Senkal B, Ince M, Yavuz E, Yaman M, Talanta, 72, 962 (2007)
Melek E, Tuzen M, Soylak M, Anal. Chim. Acta, 578, 213 (2006)
Tewari PK, Singh AK, Talanta, 56, 735 (2002)
