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Received January 14, 2014
Accepted April 1, 2014
- This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Low-cost metal oxide activated carbon prepared and modified by microwave heating method for hydrogen storage
Young Researchers and Elite Club, Islamic Azad University-Sari Branch, Sari, Iran
er_moradi@hotmail.com
Korean Journal of Chemical Engineering, September 2014, 31(9), 1651-1655(5), 10.1007/s11814-014-0096-1
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Abstract
Novel microporous activated carbon (MAC) with high surface area and pore volume has been synthesized by microwave heating. Iron oxide nanoparticles were loaded into MAC by using Fe(NO3)3·9H2O followed by microwave irradiation for up to five minutes. The surface modified microporous activated carbon was characterized by BET, XRD, SEM and thermogravimetric examinations. Adsorption data of H2 on the unmodified and modified MACs were collected with PCT method for a pressure range up to 120 bar at 303 K. Greater hydrogen adsorption was observed on the carbon adsorbents doped with 1.45 wt% of iron oxide nanoparticle loaded due to the joint properties of hydrogen adsorption on the carbon surface and the spill-over of hydrogen molecules into carbon structures.
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References
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Surya VJ, Iyakutti K, Venkataramanan N, Mizuseki H, Kawazoe Y, Int. J. Hydrog. Energy, 35(6), 2368 (2010)
Im JS, Kim SJ, Kang PH, Lee YS, J. Ind. Eng. Chem., 15(5), 699 (2009)
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Kim HS, Cha KS, Yoo BK, Ryu TG, Lee YS, Park CS, Kim YH, J. Ind. Eng. Chem., 16(1), 81 (2010)
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Hirscher M, Becher M, J. Nanosci. Nanotechnol., 3, 3 (2003)
Kim BJ, Park SJ, J. Colloid Interface Sci., 311(2), 619 (2007)
Hejazifar M, Azizian S, Sarikhani H, Li Q, Zhao D, J. Anal. Appl. Pyrol., 92, 258 (2011)
Figueroa-Torres MZ, Robau-Sanchez A, Torre-Saenz L, Aguilar-Elguezabal A, Micropor. Mesopor. Mater., 98, 89 (2007)
Dollimore D, Heal GR, J. Colloid Interface Sci.,, 33, 508 (1970)
Brunauer S, Emmett PH, Teller E, J. Am. Chem. Soc., 60, 309 (1938)
Prakash R, Fanselau K, Ren S, Manda TK, Kube C, Hahn H, Fichtner M, J. Nanotechnol., 4, 699 (2013)
Khiew P, Ho M, Tan TK, Chiu WS, Shamsudin R, Abd-Hamid MA, Chia CH, Mater. Sci. Eng., 7, 86 (2013)
Li YW, Yang RT, J. Am. Chem. Soc., 128(25), 8136 (2006)
Zacharia R, Kim KY, Kibria AKMF, Nahm KS, Chem. Phys. Lett., 412(4-6), 369 (2005)
Im JS, Yun J, Kang SC, Lee SK, Lee YS, Appl. Surf. Sci., 258(7), 2749 (2012)
Moradi SE, Amirmahmoodi S, Baniamerian MJ, J. Alloys Compd., 498, 168 (2010)
Suh MP, Park HJ, Prasad TK, Lim DW, Chem. Rev., 112(2), 782 (2012)
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