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Received May 7, 2014
Accepted September 3, 2014
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Characterization of high-alumina coal fly ash based silicate material and its adsorption performance on volatile organic compound elimination
1College of Chemical Engineering, Inner Mongolia University of Technology, Huhhot 010051, China 2Wuhai Environmental Monitoring Center, Wuhai 016000, China 3Insititute of Coal Conversion & Cyclic Economy, Inner Mongolia University of Technology, Huhhot 010051, China
tadzhang@pku.edu.cn
Korean Journal of Chemical Engineering, March 2015, 32(3), 436-445(10), 10.1007/s11814-014-0264-3
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Abstract
A highly stable silicate material from high-alumina coal fly ash was prepared and characterized using X-ray diffraction, scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy, thermal analysis, Xray photoelectron spectroscopy, and elemental analysis. The spectral results show that the silicate material was mainly composed of six elements, C, Ca, O, Si, Mg, and Al, in the form of Ca2+, Mg2+, Al3+, SiO3 2-, and CO3 2- ions. Some adsorbed water and/or water of crystallization was also observed. The silicate material showed exceptionally high capability to adsorb volatile organic compounds (VOCs). The results of dynamic adsorption behavior show that the silicate material presents similar properties with commercial activated carbon and stronger absorption properties than commercial diatomite for the adsorption of VOCs. The FTIR spectral results show weak hydrogen bonding interactions of the silicate material with three VOCs.
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References
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Spivey JJ, Ind. Eng. Chem. Res., 26, 2165 (1987)
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Qiao SZ, Bhatia SK, Nicholson D, Langmuir, 20(2), 389 (2004)
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Torralvo FA, Fernandez-Pereira C, Miner. Eng., 24, 35 (2011)
Shemi A, Mpana RN, Ndlovu S, van Dyk LD, Sibanda V, Seepe L, Miner. Eng., 34, 30 (2012)
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Zhang ZJ, Sun JM, Cao HF, Zhang XY, Wang YW, Yao Q, Patent, CN101591023 (2008)
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Sharma A, Bhattacharya A, Shrivastava A, Enzyme Microb. Technol., 48(4-5), 416 (2011)
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Zaitan H, Bianchi D, Achak O, Chafik T, J. Hazard. Mater., 153(1-2), 852 (2008)
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Guillemot A, Mijoin J, Mignard S, Magnoux P, Appl. Catal. B: Environ., 75(3-4), 249 (2007)
Jiun-Horng T, Hsiu-Mei C, Guan-Yinag H, Hung-Lung C, J. Hazard. Mater., 154(1-3), 1183 (2008)
