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In relation to this article, we declare that there is no conflict of interest.
Publication history
Received August 26, 2015
Accepted December 11, 2015
articles This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Preparation of γ-alumina nanoparticle modified polyacrylamide composite and study on its solid phase extraction of Sunset Yellow

Department of Chemistry and Chemical Engineering, Taiyuan Institute of Technology, Taiyuan 030008, P. R. China 1College of Chemistry, Jilin University, Changchun 130012, P. R. China 2State Key Laboratory of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun 130012, P. R. China
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Korean Journal of Chemical Engineering, April 2016, 33(4), 1337-1344(8), 10.1007/s11814-015-0279-4
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Abstract

An organic-inorganic composite, γ-alumina nanoparticle modified polyacrylamide, was synthesized in this study. The composite was characterized by scanning electron microscope, nitrogen adsorption-desorption measurement, thermal gravimetric analyzer, differential scanning calorimetry, and Fourier-transformed infrared spectrometer. A novel solid-phase extraction method with the synthesized composite as the adsorbent was developed for the enrichment of Sunset Yellow coupled with ultraviolet-visible spectrophotometry. To obtain the optimum extraction efficiency, the experimental parameters in the processes of preparation of the adsorbent and solid-phase extraction were studied including synthesis temperature, synthesis time, the dosage of γ-alumina nanoparticles, sample flow rate, sample pH, eluant concentration, and eluant flow rate. Under the optimum conditions, the detection limit of the developed method was calculated to be 0.037 μg mL-1 with intra-day and inter-day relative standard deviation values of 2.57% and 3.89%, respectively. When the method was applied to the determination of Sunset Yellow in beverages, satisfactory recoveries were obtained in the range of 92.3-109.8%.

References

Minioti KS, Sakellariou CF, Thomaidis NS, Anal. Chim. Acta, 583, 103 (2007)
Golka K, Kopps S, Myslak ZW, Toxicol. Lett., 151, 203 (2004)
GB 2760-2011, Hygiene standards for use of food additives, Health Ministry of P. R. China, Beijing (2011).
Li WJ, Zhou X, Tong SS, Jia Q, Talanta, 105, 386 (2013)
Gao HG, Gong WJ, Zhao YG, Anal. Sci., 31, 205 (2015)
Zhang J, Wang M, Chao S, Wang W, He Y, Chen Z, J. Electroanal. Chem., 685, 47 (2012)
Vidotti EC, Cancino JC, Oliveira CC, Rollemberg MCE, Anal. Sci., 21, 149 (2005)
Djafarzadeh N, Safarpour M, Khataee A, Korean J. Chem. Eng., 31(5), 785 (2014)
Qi R, Zhou X, Li X, Ma J, Lu C, Mu J, Zhang X, Jia Q, Analyst, 139, 6168 (2014)
Fuh MR, Chia KJ, Talanta, 56, 663 (2002)
Liu W, Zhao WJ, Chen JB, Yang MM, Anal. Chim. Acta, 605, 41 (2007)
Wang Y, Mei M, Huang X, Yuan D, Anal. Methods, 7, 551 (2015)
Hu X, Cai Q, Fan Y, Ye T, Cao Y, Guo C, J. Chromatogr. A, 1219, 39 (2012)
Yu X, Sun Y, Jiang CZ, Gao Y, Wang YP, Zhang HQ, Song DQ, J. Sep. Sci., 35, 3403 (2012)
Xin J, Zhao D, Zhang L, Xu Z, Zhou J, Qu D, Chromatographia, 73, 235 (2011)
Su R, Zhao X, Li Z, Jia Q, Liu P, Jia J, Anal. Chim. Acta, 676, 103 (2010)
Naraghi K, Panahi HA, Hassani AH, Moniri E, Korean J. Chem. Eng., 31(10), 1818 (2014)
Ye J, Liu S, Tian M, Li W, Hu B, Zhou W, Jia Q, Talanta, 118, 231 (2014)
Geng QJ, Cui WW, Ind. Eng. Chem. Res., 49(22), 11321 (2010)
Mahmoudi K, Hosni K, Hamdi N, Srasra E, Korean J. Chem. Eng., 32(2), 274 (2015)
Wang YR, Chu W, Ind. Eng. Chem. Res., 50(14), 8734 (2011)
Roh J, Umh HN, Yoo CM, Rengaraj S, Lee B, Kim Y, Korean J. Chem. Eng., 29(7), 903 (2012)
Al-Degs YS, El-Sheikh AH, Al-Ghouti MA, Hemmateenejad B, Walker GM, Talanta, 75, 904 (2008)
Xu Z, Zhang Q, Fang HHP, Crit. Rev. Environ. Sci. Technol., 33, 363 (2003)
Guan Y, Mao YH, Wei D, Wang XX, Zhu PX, Korean J. Chem. Eng., 30(9), 1810 (2013)
Ye JJ, Feng W, Tian MM, Zhang JL, Zhou WH, Jia Q, Anal. Methods, 5, 1046 (2013)
Senkal BF, Yavuz E, Polym. Adv. Technol., 17, 928 (2006)
Hashem A, Abdel-Halim ES, Socker HH, Polym. Plast. Tech. Eng., 46, 71 (2007)
Fanta GF, Burr RC, Russell CR, Rist CE, J. Appl. Polym. Sci., 10, 929 (1966)
Wu MH, Wu RA, Zhang ZB, Zou HF, Electrophoresis, 32(1), 105 (2011)
Ahmad R, Kumar R, Clean: Soil, Air, Water, 39, 74 (2011)
Krenkova J, Foret F, J. Sep. Sci., 34, 2106 (2011)
Tong S, Liu Q, Li Y, Zhou W, Jia Q, Duan T, J. Chromatogr. A, 1253, 22 (2012)
Kujawa J, Kujawski W, Koter S, Rozicka A, Cerneaux S, Persin M, Larbot A, Colloids Surf. A: Physicochem. Eng. Asp., 420, 64 (2013)
Meder F, Daberkow T, Treccani L, Wilhelm M, Schowalter M, Rosenauer A, Maler L, Rezwan K, Acta Biomater., 8, 1221 (2012)
Tian M, Feng W, Ye J, Jia Q, Anal. Methods, 5, 3984 (2013)
Chen YJ, Jing RZ, Cheng SC, Wang YH, Wan QJ, Xiong LY, He ZF, J. GuiZhou Agric. Coll., 15, 66 (1996)
Xie SF, Svec F, Frechet JM, J. Polym. Sci. A: Polym. Chem., 35(6), 1013 (1997)
Svec F, Frechet JMJ, Chem. Mater., 7, 707 (1995)
Shek CH, Lai JKL, Gu TS, Lin GM, Nanostruct. Mater., 8, 605 (1997)
Yoshioka N, Ichihashi K, Talanta, 74, 1408 (2008)
Alves SP, Brum DM, de Andrade ECB, Netto ADP, Food Chem., 107, 489 (2008)
Ma M, Luo XB, Chen B, Sub SP, Yao SZ, J. Chromatogr. A, 1103, 170 (2006)

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