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- In relation to this article, we declare that there is no conflict of interest.
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Received July 1, 2016
Accepted December 27, 2016
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Facile synthesis of imprinted submicroparticles blend polyvinylidene fluoride membranes at ambient temperature for selective adsorption of methyl p-hydroxybenzoate
School of Chemistry and Chemical Engineering, Jiangsu University, Zhenjiang 212013, China
Korean Journal of Chemical Engineering, March 2017, 34(3), 600-608(9), 10.1007/s11814-016-0365-2
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Abstract
We developed a simple phase inversion technique to prepare molecularly imprinted membrane (MIM) at room temperature for membrane selective adsorption and separation of methyl p-hydroxybenzoate (M4HB). The prepared SMIP-MIM was characterized by SEM, FT-IR, TGA. Compared with non-imprinted membrane (NIM1-5) adsorbent, SMIP-MIM1-5 adsorbent with high specific surface area and showed higher binding capacity, faster kinetic and better selectively adsorption capacity for M4HB. The maximum isotherm adsorption capacity for M4HB of SMIPMIM4 was 3.519mg·g-1, and the experimental data was well fitted to the slips model by multiple analysis. The maximum kinetic adsorption capacity and equilibrium adsorption time for SMIP-MIM4 were 1.335mg·g-1 and 160 min, respectively. The mechanism for dynamic adsorption of M4HB onto SMIP-MIM4 was found to follow pseudo-firstorder model and pseudo-second-order model. Additionally, the permeability separation factor of SMIP-MIM4 for M4HB compared to a structural analogues methyl 2-hydroxybenzoate (M2HB) could reach 2.847. The adsorption capacity of SMIP-MIM4 for M4HB and M2HB was 0.549mg·cm.2 and 1.563mg·cm-2, respectively. The adsorption behavior of M4HB through SMIP-MIM4 followed the retarded permeation mechanism.
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References
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Wang DL, Li K, Teo WK, J. Membr. Sci., 163(2), 211 (1999)
Abed MRM, Kumbharkar SC, Groth AM, Li K, Sep. Purif. Technol., 106, 47 (2013)
Meng MJ, Wang ZP, Ma LL, Zhang M, Wang J, Dai XH, Yan YS, Ind. Eng. Chem. Res., 51(45), 14915 (2012)
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He ZH, Meng MJ, Yan L, Zhu WH, Sun FQ, Yan YS, Liu Y, Liu SJ, Sep. Purif. Technol., 145, 63 (2015)
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Baydemir G, Andac M, Bereli N, Say R, Denizli A, Ind. Eng. Chem. Res., 46(9), 2843 (2007)
Ulbricht M, J. Chromatogr. B, 804, 113 (2004)
