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Received July 13, 2016
Accepted November 29, 2016
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Effect of process parameters on the CaCO3 production in the single process for carbon capture and mineralization
Arti Murnandari1 2
Jimin Kang1 3
Min Hye Youn1 4
Ki Tae Park1 4
Hak Joo Kim1 4
Seong-Pil Kang1 4
Soon Kwan Jeong1 2†
1Green Energy Process Laboratory, Korea Institute of Energy Research, 152 Gajeong-ro, Yuseong-gu, Daejeon 34128, Korea 2University of Science and Technology Korea, 217 Gajeong-ro, Yuseong-gu, Daejeon 34129, Korea 3Department of Chemical and Biological Engineering, Korea University, 145, Anam-ro, Sungbuk-gu, Seoul 02841, Korea 4, Korea
jeongsk@kier.re.kr
Korean Journal of Chemical Engineering, March 2017, 34(3), 935-941(7), 10.1007/s11814-016-0340-y
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Abstract
The regeneration of the CO2 capture system is the most energy-intensive process associated with CO2 capture because high temperatures are required to desorb CO2 from the absorbent. We propose a single process for effective CO2 capture and mineralization as a substitute for desorption of absorbed CO2, producing high value-added CaCO3. A saturated 2-amino-2-methyl-1-propanol (AMP) solution was used as a carbonate source, and calcium chloride (CaCl2) was used as a calcium ion source to precipitate CaCO3. A semi-batch reactor was used to investigate the effects of the mixing rate, temperature, and amount of calcium added during the CaCO3 precipitation process. During the mineralization reaction, the absorbed CO2 in AMP solution instantly converted into white CaCO3 precipitant with 97.4% conversion. The stirring rate provided a reciprocal effect on the crystal size, whereas the temperature and Ca/CO2 molar ratio appeared to affect the crystal morphology.
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Popescu MA, Isopescu R, Matei C, Fagarasan G, Plesu V, Adv. Powder Technol., 25(2), 500 (2014)
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Carmona JG, Morales JG, Clemente RR, J. Colloid Interface Sci., 261(2), 434 (2003)
Ukrainczyk M, Kontrec J, Babic-Ivancic V, Brecevic L, Kralj D, Powder Technol., 171(3), 192 (2007)
Feng B, Yong AK, An H, Mater. Sci. Eng., 445, 170 (2007)
Vucak M, Peric J, Pons MN, Chanel S, Powder Technol., 101(1), 1 (1999)
Prah J, Macek J, Drazic G, J. Cryst. Growth, 324(1), 229 (2011)
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Torbacke M, Rasmuson AC, AIChE J., 50(12), 3107 (2004)
Beck R, Andreassen JP, AIChE J., 58(1), 107 (2012)
Kitamura M, Cryst. Eng. Comm., 11, 949 (2009)
Lopez-Periago AM, Pacciani R, Garcia-Gonzalez C, Vega LF, Domingo C, J. Supercrit. Fluids, 52(3), 298 (2010)
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Schlomach J, Quarch K, Kind M, Chem. Eng. Technol., 29(2), 215 (2006)
Keith HD, Padden FJ, J. Appl. Phys., 34, 2409 (1963)
Ahn JW, Kim JH, Park HS, Kim JA, Han C, Kim H, Korean J. Chem. Eng., 22(6), 852 (2005)
Jung T, Kim W, Choi CK, Cryst. Res. Technol., 40, 586 (2005)
Han YS, Hadiko G, Fuji M, Takahashi M, J. Cryst. Growth, 276(3-4), 541 (2005)
Sohnel O, Mullin JW, J. Cryst. Growth, 60, 239 (1982)
Onimisi JA, Ismail R, Ariffin KS, Baharun N, Hussin HB, Korean J. Chem. Eng., 33(9), 2756 (2016)
