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Received November 7, 2016
Accepted February 27, 2017
- This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Purification of Chinese herbal extract with chitosan hydrochloride: Flocculation of single impurity and flocculation mechanism
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China 1College of Mechanical Engineering, Tianjin University of Science and Technology, Tianjin 300222, China
Korean Journal of Chemical Engineering, June 2017, 34(6), 1756-1762(7), 10.1007/s11814-017-0055-8
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Abstract
Chitosan hydrochloride (CHC) was used for flocculation of impurities (tannin and protein) in Ma-xinggan-shi solution (MSS), which is a Chinese herbal medicine solution (CHMS). To study the flocculation mechanism, simulated solutions of pure tannin and pure protein in water flocculated by CHC were investigated. For MSS flocculation by CHC, flocculation performance was assessed in terms of suspended turbidity, impurities removal rate as well as active components retention rate. CHC showed high capability of maintaining a low turbidity over a wide range of the polymer dosage. The optimum dosage of CHC was 0.6 g/L in base of different solution turbidity, and it also demonstrated the retention rate of total soluble polysaccharide (TSP) and ephedrine reached 78.4% and 92%, respectively.
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Fan MH, Xu SY, Sep. Purif. Technol., 61(2), 211 (2008)
Ru-An C, Fang Z, Huang K, Zhang YF, Chin. J. Nat. Med., 9, 120 (2011)
Yang Z, Yan H, Yang H, Li H, Li A, Cheng R, Water Res., 47, 3037 (2013)
Wang C, Shang C, Chen GH, Zhu XS, J. Colloid Interface Sci., 411, 213 (2013)
Tasdemir T, Kurama H, Environ. Prog. Sustain. Energy, 32, 317 (2013)
Nasser MS, Twaiq FA, Onaizi SA, Sep. Purif. Technol., 103, 43 (2013)
Verma AK, Dash RR, Bhunia P, J. Environ. Manage., 93, 154 (2012)
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Ramavandi B, Farjadfard S, Korean J. Chem. Eng., 31(1), 81 (2014)
Liu J, Tian Y, An X, Li G, Kang Y, J. Dispersion Sci. Technol., 36, 1612 (2015)
Qin L, Liu J, Li G, Kang Y, J. Dispersion Sci. Technol., 36, 695 (2015)
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Seyfarth F, Schliemann S, Elsner P, Hipler UC, Int. J. Pharm., 353, 139 (2008)
Falcao L, Araujo MEM, J. Cult. Herit., 14, 499 (2013)
Anitha A, Divya Rani VV, Krishna R, Sreeja V, Selvamurugan N, Nair SV, Tamura H, Jayakumar R, Carbohydr. Polym., 78, 672 (2009)
Guerrero P, Hanani ZAN, Kerry JP, de la Caba K, J. Food Eng., 107(1), 41 (2011)
Denavi GA, Perez-Mateos M, Anon MC, Montero P, Mauri AN, Gomez-Guillen MC, Food Hydrocolloids, 23, 2094 (2009)
Su JF, Huang Z, Yuan XY, Wang XY, Li M, Carbohydr. Polym., 79, 145 (2010)
Zhang B, Wang DF, Li HY, Xu Y, Zhang L, Ind. Crop. Prod., 29, 541 (2009)
An JH, Dultz S, App. Clay Sci., 36, 256 (2007)
Becker AL, Henzler K, Welsch N, Ballauff M, Borisov O, Curr. Opin. Colloid Interface Sci., 17, 90 (2012)
Jaramillo DP, Roberts RF, Coupland JN, Food Res. Int., 44, 911 (2011)
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Yuan Y, Wan ZL, Yang XQ, Yin SW, Food Res. Int., 55, 207 (2014)