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Received December 21, 2017
Accepted July 18, 2018
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Determination and correlation of the solubility of L-arabinose and D-galactose in binary solvent mixtures from 278.15 to 333.15 K
Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China
baozb@zju.edu.cn
Korean Journal of Chemical Engineering, October 2018, 35(10), 2043-2051(9), 10.1007/s11814-018-0116-7
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Abstract
L-arabinose and D-galactose could be released during the hydrolysis process of Arabic gum. The development of a crystallization process of L-arabinose is highly dependent on the knowledge of the solubility of both saccharides. In this work, the solubility of L-arabinose and D-galactose in binary mixtures of methanol-water or ethanolwater (mole fraction of water ≤ 0.5816) was determined at temperatures between 278.15 and 333.15 K by a static equilibrium method. The experimental data correlated well with the modified Apelblat equation, the simplified polynomial empirical equation, NRTL model and UNIQUAC model. Additionally, the thermodynamic properties including the dissolution enthalpy and entropy were obtained from the experimental data. Within the studied temperature range, the dissolution is endothermic and the dissolution process is non-spontaneous.
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