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Received April 26, 2018
Accepted July 26, 2018
- This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Surface treatment of sol-gel bioglass using dielectric barrier discharge plasma to enhance growth of hydroxyapatite
Islam El-Sayed Soliman1†
Asem El-Sayed Metawa2 3
Mohamed Abdel Hameed Aboelnasr1
Khairy Tohamy Eraba1
1Biophysics Branch, Faculty of Science, Al-Azhar University, Nasr City 11884, Cairo, Egypt 2Physics Department, Faculty of Science, Al-Azhar University, Nasr City 11884, Cairo, Egypt 3Physics Department, Faculty of Science, Al-Baha University, Al-Baha, Saudi Arabia
Korean Journal of Chemical Engineering, December 2018, 35(12), 2452-2463(12), 10.1007/s11814-018-0131-8
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Abstract
Surface treatment of sol-gel bioglass is required to increase its biomedical applications. In this study, a dielectric barrier discharge (DBD) plasma treatment in atmospheric pressure was performed on the surface of [SiO2- CaO-P2O5-B2O3] sol-gel derived glass. The obtained bioglass was treated by plasma using discharge current 12mA with an exposure period for 30 min. The type of discharge can be characterized by measuring the discharge current and applied potential waveform and the power dissipation. Apatite formation on the surface of the DBD-treated and untreated samples after soaking in simulated body fluid (SBF) at 37 °C is characterized by Fourier transform infrared spectroscopy (FTIR), X-Ray diffraction (XRD), inductively coupled plasma (ICP-OES) and scanning electron microscopy coupled with energy dispersive spectroscopy (SEM/EDS). We observed a marked increase in the amount of apatite deposited on the surface of the treated plasma samples than those of the untreated ones, indicating that DBD plasma treatment is an efficient method and capable of modifying the surface of glass beside effectively transforming it into highly bioactive materials.
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Maria VR, Ramila A, Chem. Mater., 12, 961 (2000)