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Received February 25, 2017
Accepted November 5, 2017
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Physicochemical analysis of linear low-density polyethylene composite films containing chemically treated rice husk
Korea Institute of Industrial Technology, 89 Yangdaegiro-gil, Ipjang-myeon, Seobuk-gu, Cheonan-si, Chungcheongnam-do 31056, Korea 1Department of Chemical Engineering, Yonsei University, 134 Shinchon-dong, Seodaemoon-gu, Seoul 03722, Korea
Korean Journal of Chemical Engineering, February 2018, 35(2), 594-601(8), 10.1007/s11814-017-0304-x
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Abstract
A study was conducted to determine the appropriate surface treatment for rice husks (RH) in polymer composite film to improve the physical properties relative to those of untreated RH/linear low-density polyethylene (LLDPE) film. Pulverized RH was treated with NaOH (RH-m) and acetic acid (RH-ac) to prepare composite films with LLDPE resin. The treated RH showed typical mercerization and acetylation, as confirmed by spectroscopic and thermal analysis methods. The RH-m sample was mercerized, allowing decomposition of hemicellulose and partially amorphous cellulose. The RH-ac sample was processed via acetylation inducing partial lignin decomposition. Fieldemission scanning electron microscopy showed smaller gaps at the RH/LLDPE interface for RH-m and RH-ac compared to that with untreated RH, implying increased composite compatibility. RH-m in particular showed superior tensile strength (15.85 N/mm2), elongation (884%), Young’s modulus (60.01 N/mm2), and tear strength (7.71N/mm2) compared to untreated RH and RH-ac.
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Yoon SJ, Son YI, Kim YK, Lee JG, Renew. Energy, 42, 163 (2012)
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Chen RS, Ghani MHA, Salleh MN, Ahmad S, Tarawneh MAA, J. Appl. Polym. Sci., 132 (2015)
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Kono H, Oka C, Kishimoto R, Fujita S, Carbohydr. Polym., 170, 23 (2017)
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Peters PWM, Hemptenmacher J, Schurmann H, Combust. Sci. Technol., 70, 1321 (2010)
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Fahma F, Iwamoto S, Hori N, Iwata T, Takemura A, Cellulose, 18, 443 (2010)
Salmah H, Amri F, Kamarudin H, Polym. -Plast. Technol. Eng., 51, 86 (2012)
Morsi SM, Pakzad A, Amin A, Yassar RS, Heiden PA, J. Colloid Interface Sci., 360(2), 377 (2011)
Simon M, Brostaux Y, Vanderghem C, Jourez B, Paquot M, Richel A, J. Chem. Technol. Biotechnol., 89(1), 128 (2014)
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Genieva SD, Turmanova SC, Dimitrova AS, Vlaev LT, J. Therm. Anal. Calorim., 93, 387 (2008)
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Das AM, Ali AA, Hazarika MP, Carbohydr. Polym., 112, 342 (2014)
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Trubetskaya A, Jensen PA, Jensen AD, Steibel M, Spliethoff H, Glarborg P, Larsen FH, Biomass Bioenerg., 86, 76 (2016)
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Tarley CRT, Ferreira SLC, Arruda MAZ, Microchem J., 77, 163 (2004)
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Yang HP, Yan R, Chen HP, Lee DH, Zheng CG, Fuel, 86(12-13), 1781 (2007)
