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Received April 19, 2017
Accepted December 1, 2017
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Agomelatine co-crystals with resorcinol and hydroquinone: Preparation and characterization
Min-Jeong Lee1
Nan-Hee Chun2
Hyo-Cheol Kim3
Moon-Jip Kim3
Paul Kim4
Min-Yong Cho4
Guang Jin Choi4 5†
1Crystallization and Particle Science, Institute of Chemical and Engineering Sciences, A*STAR (Agency for Science, Technology and Research), 1 Pesek Road, Jurong Island 627833, Singapore 2Unimed Pharm Inc., Asan, Chungnam 31501, Korea 3Department of Physics, Soonchunhyang University, Asan, Chungnam 31538, Korea 4Department of Pharmaceutical Engineering, Soonchunhyang University, Asan, Chungnam 31538, Korea 5Department of Medical Science, Soonchunhyang University, Asan, Chungnam 31538, Korea
guangchoi@sch.ac.kr
Korean Journal of Chemical Engineering, April 2018, 35(4), 984-993(10), 10.1007/s11814-017-0331-7
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Abstract
Perovskite type BiFeO3 (BFO) was synthesized by sol-gel auto-combustion method. Synthesized BFO was immobilized on the micro slides glass plates by sol-gel dip-coating method. The sample was characterized by XRD, FESEM, UV-Vis DRS, and BET techniques. The XRD pattern confirmed the perovskite structure, and from the Debye- Scherrer equation the average crystalline size was calculated as 19 nm. The FE-SEM images of prepared BFO showed porous structure with low agglomeration. The band gap energy was calculated about 2.13 eV, and the specific surface area (SSA) of prepared BFO nanostructure was obtained 55.1m2 g-1. The photocatalytic activity of prepared pure and immobilized BFO was investigated in the removal of NOx under UV irradiation, in the batch photoreactor. The effects of operational parameters such as initial concentration of NOx, light intensity and amount of coated photocatalyst, under identical conditions, were investigated. The results showed that the highest conversion of NOx was obtained as 35.83% in the 5 ppm of NOx with 1.2 g immobilized BFO and under 15 W illumination lamp.
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