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Received May 9, 2017
Accepted February 7, 2018
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Gd3+ doped Fe3O4 nanoparticles with proper magnetic and supercapacitive characteristics: A novel synthesis platform and characterization
1Materials and Nuclear Research School, NSTRI, P. O. Box 14395-834, Tehran, Iran 2Department of Physics, Bonab Branch, Islamic Azad University, Bonab, Iran 3Center of Excellence in Electrochemistry, Faculty of Chemistry, University of Tehran, Tehran, Iran 4Biosensor Research Center, Endocrinology and Metabolism Molecular-Cellular Sciences Institute, Tehran University of Medical Sciences, Tehran, Iran
maghazadeh@aeoi.org.ir, mustafa.aghazadeh@gmail.com
Korean Journal of Chemical Engineering, June 2018, 35(6), 1341-1347(7), 10.1007/s11814-018-0027-7
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Abstract
A novel electrochemical procedure was developed for the facile preparation of Gd-doped iron oxide nanoparticles (GdIO-NPs). A simple galvanostatic deposition (i=10mA cm-2) was done in an additive-free aqueous solution containing FeCl2·4H2O, Fe(NO3)3·9H2O and GdCl3·6H2O. The XRD, FE-SEM, EDS and TEM characterizations showed that the product is composed of 15% GdIO-NPs with 10 nm in size. VSM analysis proved that the GdIONPs are superparamagnetic. The cyclic voltammetry and charge-discharge tests showed that the prepared GdIO-NPs are capable to deliver specific capacity as high as 190.1 F g-1 at 0.5A g-1 and capacity retention of 95.1% after 2000 cycling. Based on the results, it was concluded that the developed electrochemical strategy acts as an efficient procedure for the preparation of lanthanide doped MNPs with proper magnetic and supercapacitive characters.
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References
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Aghazadeh M, Maragheh MG, Ganjali MR, Norouzi P, Faridbod F, Appl. Surf. Sci., 364, 141 (2016)
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Jin EM, Lee HJ, Jun HB, Jeong SM, Korean J. Chem. Eng., 34, 891 (2017)
Aghazadeh M, Barmi AAM, Gharailou D, Peyrovi MH, Sabour B, Khosroshahi FN, Appl. Surf. Sci., 283, 871 (2013)
Jeong GH, Lee HM, Lee H, Kim CK, Piao Y, Lee JH, Kim JH, Kim SW, RSC Adv., 4, 51619 (2014)
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Aghazadeh M, Ganjali MR, J. Mater. Sci.: Mater. Electron., 28, 11406 (2017)
Mehrabad JT, Aghazadeh M, Maragheh MG, Ganjali MR, Mater. Lett., 184, 223 (2016)
Aghazadeh M, Rashidi A, Ganjali MR, Electronic. Mater. Lett., 14, 37 (2018)
Gou JX, Xie SL, Liu YR, Liu CG, Electrochim. Acta, 210, 915 (2016)
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Aghazadeh M, Karimzadeh I, Ganjali MR, J. Mater. Sci.: Mater. Electron., 28, 18121 (2017)
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Aghazadeh M, Karimzadeh I, Ganjali MR, Mater. Lett., 209, 450 (2017)
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Tang X, Jia R, Zhai T, Xia H, ACS Appl. Mater. Interfaces, 7, 27518 (2015)
Xia T, Xu XL, Wang JP, Xu CB, Meng FC, Shi Z, Lian J, Bassat JM, Electrochim. Acta, 160, 114 (2015)
Zhang WM, Wu XL, Hu JS, Guo YG, Wan LJ, Adv. Funct. Mater., 18(24), 3941 (2008)
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Park JC, Yeo S, Kim M, Lee GT, Seo JH, Mater. Lett., 181, 272 (2016)
Zhang H, Malik V, Mallapragada S, Akinc M, J. Magn. Magn. Mater., 423, 386 (2017)
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Aghazadeh M, Ganjali MR, J. Mater. Sci.: Mater. Electron., 29, 4981 (2018)
Karimzadeh I, Aghazadeh M, Ganjali MR, Dourudi T, Curr. Nanosci., 13, 167 (2017)
Karimzadeh I, Dizaji HR, Aghazadeh M, Mater. Res. Express, 3, 095022 (2016)
Aghazadeh M, Ganjali M, J. Mater. Sci., 53(1), 295 (2018)
Bakhtiary Z, Saei AA, Hajioour MJ, Raoufi M, Vermesh O, Mahmoudi M, Nanomed., 12, 287 (2016)
Ulbrich K, Hola K, Subr V, Bakandritsos A, Tucek J, Zboril R, Chem. Rev., 116(9), 5338 (2016)
