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Received April 9, 2019
Accepted August 9, 2019
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Synthesis of bi-functionalized ionic liquid - mesoporous alumina composite material and its CO2 capture capacity
1Key Laboratory for Green Chemical Technology of Ministry of Education, School of Chemical Engineering & Technology, Tianjin University, Tianjin 300350, China 2Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Tianjin University, Tianjin 300072, China
shktang@tju.edu.cn
Korean Journal of Chemical Engineering, October 2019, 36(10), 1708-1715(8), 10.1007/s11814-019-0360-5
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Abstract
Bi-functionalized ionic liquid (IL) - mesoporous alumina (MA) composite material was synthesized and used for CO2 capture. Ordered mesoporous alumina was synthesized by self-assembly method with aluminum isopropoxide as aluminum source. Then bi-functionalized ionic liquid 1-methoxyethyl-3-methyl imidazole glycinate ([MOEmim][Gly]) was immobilized on mesoporous alumina by ultrasonic-assisted impregnation method. Ordered mesostructure of alumina keeps well in the composite material. Compared with bi-functionalized ionic liquid, thermal stability of the composite material greatly improved. Finally, CO2 capture capacity of IL-MA composite material was studied under different temperatures. On the basis of both capture capacity and capture rate, 40 °C is the optimal temperature. The capture capacity is 1.42mol·mol IL-1 - equivalent to 144mg·g sorbent-1, which is higher than IL or MA alone. Furthermore, the capture capacity of composite material almost maintains constant after eight capture-regeneration cycles.
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