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Received August 4, 2018
Accepted December 2, 2018
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Quantification of recalcitrant organic compounds during their removal test by a novel and economical method based on chemical oxygen demand analysis
Abraham Efraim Rodriguez-Mata
Leonel Ernesto Amabilis-Sosa†
Adriana Roé-Sosa1
Jose Manuel Barrera-Andrade2
Jesús Gabriel Rangel-Peraza3
and María G. Salinas-Juárez4
CONACyT-Instituto Tecnologico de Culiacan, Juan de Dios Bátiz 310, C.P. 80220, Culiacán, Sinaloa, Mexico 1Universidad Tecnológica de Culiacán, Carretera Imala km 2, C.P. 80014, Culiacán, Sinaloa, México, Mexico 2Escuela Superior de Ingeniería Química e Industrias Extractivas, Instituto Politécnico Nacional, Mexico City, Mexico, Korea 3División de Estudios de Posgrado e Investigación, Tecnológico Nacional de México-Instituto Tecnológico de Culiacán, Sinaloa, México, Mexico 4Departamento de Ingeniería Química, Facultad de Estudios Superiores Zaragoza, UNAM, México, Mexico
Korean Journal of Chemical Engineering, March 2019, 36(3), 423-432(10), 10.1007/s11814-018-0203-9
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Abstract
This article proposes the use of mathematical models obtained by the Pearson correlation between the concentration of various recalcitrant organic compounds (ROCs) measured by chromatographic analysis (ChrA) and experimental chemical oxygen demand (COD). The aim is to reduce the number of samples processed by the ChrA, diminishing the economic costs of analysis. Ten ROCs, including pesticides, colorants, aromatic hydrocarbons and pharmaceuticals compounds, were introduced into four advanced oxidation processes operated at different residence times. Every ROC was tested at each residence time by COD determination and by quantification of concentrations with ChrA. Furthermore, chemical equations for the COD reaction of every ROC were formulated. A linear model was obtained for all the ROCs, after corroborating that the correlation between theoretical and experimental COD was >0.99, which established the ROC concentration from the experimental COD, omitting the ChrA. Results indicated that it is possible to know concentrations in most of the ROCs by means of the experimental COD with a >99±0.01% of accuracy, which leads to a cost decrease and even to evaluate methods in developing countries, which often do not have chromatographs and where pollution issues are meaningful.
Keywords
References
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