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Received February 11, 2019
Accepted July 15, 2019
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Fluorescence detection of bisphenol A in aqueous solution using magnetite core-shell material with gold nanoclusters prepared by molecular imprinting technique
Department of Chemical Engineering, Keimyung University, 1095 Dalgubeoldaero, Dalseo-gu, Daegu 42601, Korea
leeb@kmu.ac.kr
Korean Journal of Chemical Engineering, September 2019, 36(9), 1509-1517(9), 10.1007/s11814-019-0342-7
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Abstract
Technologies for detecting endocrine disrupting compounds such as bisphenol A (BPA) in an aqueous solution in a convenient way and low cost have gained much attention. In this work, to overcome the drawbacks of current detection methods, we applied molecular imprinted polymers (MIPs) to core-shell materials. The core-shell material has the advantage that both properties of the core and shell materials can be used simultaneously. After binding BPA in an aqueous solution, the magnetic core material was able to be recovered using magnetism. In addition, functional groups were easily introduced using silica as a shell material. Gold nanoclusters (AuNCs) and MIPs were used to give changes in the fluorescence intensity when BPA was bound to the prepared core-shell material. The physical properties of the prepared Fe3O4@SiO2@AuNCs-MIP (CS-MIP) were analyzed and fluorescence intensities of CSMIP for BPA were examined. The prepared material was recovered using a magnet, and the recovered CS-MIP was regenerated to investigate how the fluorescence properties for BPA changed in the subsequent reuses.
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Kim YH, Lee B, Choo KH, Choi SJ, Microporous Mesoporous Mater., 185, 121 (2014)
