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Received August 11, 2019
Accepted December 1, 2019
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Microwave assistant production of a high performance adsorbent from rice husk
Department of Physical Chemistry, Faculty of Chemistry, University of Kashan, Kashan, Iran
Korean Journal of Chemical Engineering, February 2020, 37(2), 240-248(9), 10.1007/s11814-019-0446-0
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Abstract
Microwave radiation was used for synthesis of an adsorbent using rice husk. The activation of the rice husk sample was performed by H3PO4 and 6min of the microwave radiation with power 700W. The synthesized adsorbent was characterized by SEM, FT-IR, BET and XRD techniques. These analyses showed the prepared adsorbent is an amorphous and mesoporous nano-adsorbent with BET surface area 276.43m2/g. It has some aromatic groups and O-H, C=C, C.O and C=O bands in its structure. Adsorption of alizarin yellow on the synthesized nano-adsorbent was investigated and the influences of adsorbent dosage (0.1-2 g/L) and temperature (25-40 °C) on dye removal from aqueous solution were investigated. The kinetic, equilibrium and thermodynamics studies of alizarin yellow removal from aqueous solution using the prepared adsorbent were carried out. The adsorption performance of alizarin yellow on the prepared adsorbent was compared with a commercial activated carbon. The importance of this study is in providing a condition for preparation of a low cost adsorbent with high adsorption capacity (712.63 mg/g) for alizarin yellow. The comparison of adsorption capacities of the prepared adsorbent from rice husk and other adsorbents proved it is a perfect adsorbent.
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References
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Baytar O, Sahin O, Saka C, Appl. Therm. Eng., 138, 542 (2018)
Baytar O, SAhin O, Saka C, Agrak S, Anal. Lett., 51, 2205 (2018)
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Chen Y, Zhai SR, Liu N, Song Y, An QD, Song XW, Bioresour. Technol., 144, 401 (2013)
Eris S, Bashiri H, Prog. React. Kinet. Mech., 41, 109 (2016)
Freundlich H, Z. Phys. Chem., 57U, 385 (1907)
Gholivand M, Yamini Y, Dayeni M, Seidi S, Tahmasebi E, J. Environ. Chem. Eng., 3, 529 (2015)
Gupta VK, Mittal A, Jain R, Mathur M, Sikarwar S, J. Colloid Interface Sci., 303(1), 80 (2006)
Hameed BH, Salman JM, Ahmad AL, J. Hazard. Mater., 163(1), 121 (2009)
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Ho YS, J. Hazard. Mater., 136(3), 681 (2006)
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Izgi MS, Saka C, Baytar O, Saracoglu G, Sahin O, Anal. Lett., 52, 772 (209)
Ji YB, Li TH, Zhu L, Wang XX, Lin Q, Appl. Surf. Sci., 254(2), 506 (2007)
Khalil KMS, Allam OAS, Khairy M, Mohammed KMH, Elkhatib RM, Hamed MA, J. Mol. Liq., 247, 386 (2017)
Lagergren S, Kungliga Svenska Vetenskapsakademiens. Handlingar, 24, 1 (1898).
Narayanan AL, Dhamodaran M, Solomon JS, Int. J. Eng. Appl. Sci., 7, 36 (2015)
Langmuir I, J. Am. Chem. Soc., 38, 2221 (1916)
Lin L, Zhai SR, Xiao ZY, Song Y, An QD, Song XW, Bioresour. Technol., 136, 437 (2013)
Menendez JA, Arenillas A, Fidalgo B, Fernandez Y, Zubizarreta L, Calvo EG, Bermudez JM, Fuel Process. Technol., 91(1), 1 (2010)
Menya E, Olupot PW, Storz H, Lubwama M, Kiros Y, Chem. Eng. Res. Des., 129, 271 (2018)
Muniandy L, Adam F, Mohamed AR, Ng EP, Microporous Mesoporous Mater., 197, 316 (2014)
Parra S, Stanca SE, Guasaquillo I, Thampi KR, Appl. Catal. B: Environ., 51(2), 107 (2004)
Rahman IA, Saad B, Shaidan S, Rizal ESS, Bioresour. Technol., 96(14), 1578 (2005)
Ratan JK, Kaur M, Adiraju B, Materials Today: Proceedings, 5, 3334 (2018)
Redlich O, Peterson DL, J. Phys. Chem., 63, 1024 (1959)
Salman M, Athar M, Shafique U, Imran M, Rehman R, Akram R, Zulfiqar Ali S, Turkish J. Eng. Env. Sci., 35, 209 (2011)
Sarabadan M, Bashiri H, Mousavi SM, Clay Miner., 1, in press (2019).
Sarabadan M, Bashiri H, Mousavi SM, Korean J. Chem. Eng., 36(10), 1575 (2019)
Sharif YM, Saka C, Baytar O, Sahin O, Anal. Lett., 51, 2733 (2018)
Sips R, J. Chem. Phys., 16, 490 (1948)
Sivaraj R, Namasivayam C, Kadirvelu K, Waste Manage., 21, 105 (2001)
Soltani N, Bahrami A, Pech-Canul MI, Gonzalez LA, Chem. Eng. J., 264, 899 (2015)
Somasundaram S, Sekar K, Gupta VK, Ganesan S, J. Mol. Liq., 177, 416 (2013)
Temkin MJ, Pyzhev V, Acta Physicochim. URSS, 12, 327 (1940)
Toles CA, Marshall WE, Wartelle LH, McAloon A, Bioresour. Technol., 75(3), 197 (2000)
Tran HN, You SJ, Chao HP, J. Environ. Chem. Eng., 4, 2671 (2016)
Ugurla M, Gurses A, Acikyildiz M, Microporous Mesoporous Mater., 111, 228 (2008)
Yang JY, Jiang XY, Jiao FP, Yu JG, Appl. Surf. Sci., 436, 198 (2018)
Zeldowitsch J, Acta Physicochim. URSS, 1, 449 (1934)
Zhang J, Fu H, Lv X, Tang J, Xu X, Biomass Bioenergy, 35, 464 (2011)
Zhou Y, Zhang L, Cheng Z, J. Mol. Liq., 212, 739 (2015)
