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- In relation to this article, we declare that there is no conflict of interest.
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Received July 11, 2019
Accepted November 10, 2019
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Thin film composite polyesteramide nanofiltration membranes fabricated from carboxylated chitosan and trimesoyl chloride
College of Materials and Environmental Engineering, Hangzhou Dianzi University, Hangzhou, China 1Key Laboratory of Advanced Textile Materials and Manufacturing Technology of Education Ministry, Zhejiang Sci-Tech University, Hangzhou, China
dihuaw@hotmail.com
Korean Journal of Chemical Engineering, February 2020, 37(2), 307-321(15), 10.1007/s11814-019-0426-4
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Abstract
Thin film composite polyesteramide nanofiltration membranes were fabricated with interfacial polymerization from carboxylated chitosan and trimesoyl chloride on a microporous polysulfone support membrane. Salt rejection was improved by building a multiple-layer structure that was formed by sequentially repeating the cycles of the interfacial reactions. The chemical structure, surface morphology and charge were characterized for the polyesteramide top layer. The effects of the concentrations of the reactant solutions and the number of cycles of reactant depositions and reactions on the separation performance were investigated. The single-layer polyesteramide membrane produced from 3.5 wt% carboxylated chitosan and 0.7 wt% TMC has a negatively charged surface and shows favorable separation performance: pure water permeation flux of 7.3 L/(m2 h) at 0.6MPa gauge feed pressure, and salt rejection of 95.0% for Na2SO4, 65.7% for MgSO4, 33.2% for MgCl2 and 66.3% for NaCl. The multiple-layer polyesteramide membranes show a more negatively charged surface and higher salt rejection than the single-layer polyesteramide membranes. The single-layer polyesteramide membrane PS-[(C-CS)1.0/TMC] with a relatively loose structure shows good retention for the reactive black 5 anionic dye. This study opens an interesting research area to explore a new type of thin film composite nanofiltration membrane.
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References
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Chen GE, Liu YJ, Xu ZL, Tang YJ, Huang HH, Sun L, RSC. Adv., 5, 40742 (2015)
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Liu MH, Zheng YP, Shuai S, Zhou Q, Yu SC, Gao CJ, Desalination, 288, 98 (2012)
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Zhang Y, Su YL, Peng JM, Zhao XT, Liu JZ, Zhao JJ, Jiang ZY, J. Membr. Sci., 429, 235 (2013)
Zhao JJ, Su YL, He X, Zhao XT, Li YF, Zhang RN, Jiang ZY, J. Membr. Sci., 465, 41 (2014)
Huang YF, Sun JJ, Wu DH, Feng XS, Sep. Purif. Technol., 207, 142 (2018)
Tang YJ, Wang LJ, Xu ZL, Zhang HZ, J. Polym. Res., 25, 118 (2018)
Ma XH, Yang Z, Yao ZK, Xu ZL, Tang CYY, J. Membr. Sci., 525, 269 (2017)
Dash M, Chiellini F, Ottenbrite RM, Chiellini E, Prog. Polym. Sci, 36, 981 (2011)
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Ilyas S, de Grooth J, Nijmeijer K, de Vos WM, J. Colloid Interface Sci., 446, 386 (2015)
Cheng W, Liu CH, Tong TZ, Epsztein R, Sun M, Verduzco R, Ma J, Elimelech M, J. Membr. Sci., 559, 98 (2018)
Tang YJ, Xu ZL, Xue SM, Wei YM, Yang H, J. Membr. Sci., 541, 483 (2017)
Liu MH, Wu DH, Yu SC, Gao CJ, J. Membr. Sci., 326(1), 205 (2009)
Dizge N, Epsztein R, Cheng W, Porter CJ, Elimelech M, J. Membr. Sci., 549, 357 (2018)
Zhao CW, Yang B, Han JL, Meng YY, Yu L, Hou DY, Wang J, Zhao Y, Zhai YH, Wang SG, Sun XF, Appl. Surf. Sci., 453, 502 (2018)
Peydayesh M, Mohammadi T, Bakhtiari O, Sep. Purif. Technol., 194, 488 (2018)
Cai ZJ, Zhu C, Xiong P, Guo J, Zhao KY, J. Mater. Sci., 53(20), 14801 (2018)
