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Received March 18, 2021
Accepted June 27, 2021
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Optimization of UV-photografting factors in preparation of polyacrylic-polyethersulfone forward osmosis membrane using response surface methodology
Ahmad Fikri Hadi Abdul Rahman1
Zulsyazwan Ahmad Khushairi1
Mazrul Nizam Abu Seman1 2†
Mohamed Khayet3 4
1Faculty of Chemical and Process Engineering Technology, Universiti Malaysia Pahang, Lebuhraya Tun Razak, 26300 Gambang, Kuantan, Pahang, Malaysia 2Earth Resources and Sustainability (ERAS) Center, Universiti Malaysia Pahang, Lebuhraya Tun Razak, 26300 Gambang, Kuantan, Pahang, Malaysia 3Department of Structure of Matter, Thermal Physics and Electronics, Faculty of Physics, University Complutense of Madrid, Av. Complutense s/n, 28040, Madrid, Spain 4Madrid Institute for Advanced Studies of Water (IMDEA Water Institute), Calle Punto Net No 4 28805, Alcalá de Henares, Madrid (Spain)
Korean Journal of Chemical Engineering, November 2021, 38(11), 2313-2323(11), 10.1007/s11814-021-0881-6
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Abstract
Commercial nanofiltration polyethersulfone (NF2) membrane was modified via ultraviolet (UV) photografting to prepare a high-performance forward osmosis (FO) membrane. The optimized condition of grafting parameters was obtained using central composite design (CCD) and response surface methodology (RSM). UV-photografting time and acrylic acid (AA) monomer concentration were the considered variables, while the two RSM responses were water permeate flux and reverse salt diffusion flux (RSD). Quadratic models were established between the responses and the independent parameters using analysis of variance (ANOVA). The membranes were characterized with functional group, morphology and surface roughness. The obtained optimum conditions were 2.81min grafting time and 27.85 g/L AA monomer concentration. Under these conditions, a maximum water permeate flux of 1.52±0.04 L/m2·h was achieved with an RSD value of 10.09±0.36 g/m2·h. The optimized membrane exhibited a higher water flux compared to the unmodified NF2 membrane without any significant change of the RSD value.
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References
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Alaswad SO, Alpay SAE, Sharif AO, J. Chem. Eng. Process Technol., 09, 1 (2018)
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Abdul Rahman AFH, Abu Seman MN, J. Env. Chem. Eng., 6, 4368 (2018)
Pardeshi M, Mungray AA, Sci. Rep., 9, 1937 (2019)
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Garcia-Ivars J, Iborra-Clar MI, Alcaina-Miranda MI, Mendoza-Roca JA, Pastor-Alcaniz L, Chem. Eng. J., 283, 231 (2016)
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Abu Seman MN, Khayet M, Hilal N, Desalination, 287, 19 (2012)
Peeva PD, Pieper T, Ulbricht M, J. Membr. Sci., 362(1-2), 560 (2010)
Pieracci J, Crivello JV, Belfort G, Chem. Mater., 14(1), 256 (2002)
Rahimpour A, Desalination, 265(1-3), 93 (2011)
Taniguchi M, Belfort G, J. Membr. Sci., 231(1-2), 147 (2004)
Chung YT, Ng LY, Mohammad AW, J. Ind. Eng. Chem., 20(4), 1549 (2014)
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Zhao C, Xue J, Ran F, Sun S, Prog. Mat. Sci., 58(1), 76 (2013)
Ulbricht M, Polymer, 47(7), 2217 (2006)
Khayet M, Cojocaru C, Zakrzewska-Trznadel G, J. Membr. Sci., 321(2), 272 (2008)
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Van der Bruggen B, J. Appl. Pol. Sci., 114(1), 630 (2009)
Abuhabib AA, Mohammad AW, Hilal N, Rahman RA, Shafie AH, Desalination, 295, 16 (2012)
Law JY, Mohammad AW, Jurnal Teknologi, 79(5-3), 47 (2017)
Law JY, Mohammad AW, J. Ind. Eng. Chem., 51, 264 (2017)
Li JY, Ni ZY, Zhou ZY, Hu YX, Xu XH, Cheng LH, J. Membr. Sci., 552, 213 (2018)
Puro L, Manttari M, Pihlajamaki A, Nystrom M, Chem. Eng. Res. Des., 84(A2), 87 (2006)
