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Received March 1, 2021
Accepted May 27, 2021
- This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Electrical property improvement of phenolic formaldehyde resin with graphene and ionic liquid
Institute of Petrochemical Technology, Jilin Institute of Chemical Technology, Jilin 132022, P. R. China 1Department of Polymer Materials, Jilin Institute of Chemical Technology, Jilin City 132022, P. R. China 2Department of Chemistry, College of Science, Yanbian University, Yanji 133002, Jilin, China 3Department of Chemistry, Inha University, Michuhol-gu, Incheon 22212, Korea
jinfanlong@163.com
Korean Journal of Chemical Engineering, November 2021, 38(11), 2332-2340(9), 10.1007/s11814-021-0860-y
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Abstract
The ionic liquid 3-decyl-bis(1-vinyl-1H-imidazole-3-ium-bromide) (C10[VImBr]2) was synthesized and its chemical structure characterized by Fourier-transform infrared spectroscopy and 1H nuclear magnetic resonance spectroscopy. To improve the electrical conductivity of the phenolic formaldehyde (PF) resin, PF/graphene and PF/graphene/ C10[VImBr]2 composites were prepared via a melt blending and compression-curing process. The impact strength of the composites was shown to increase with the addition of increasing proportion of graphene, and with increasing proportion of C10[VImBr]2, of up to 5 wt%. In detail, the electrical conductivity of the PF/graphene composites increased significantly from 2.3 x 10-12 to 4 x 10-4 S/cm as the graphene content increased from 0 to 20 wt%. Moreover, the electrical conductivity of the PF/graphene/C10[VImBr]2 composites containing 15 wt% graphene was shown to increase from 5.6 x 10-5 to 9.2 x 10-4 S/cm as the content of C10[VImBr]2 increased from 0 to 5 wt%.
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