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Received April 18, 2021
Accepted August 8, 2021
- This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
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Purification of durene from the mixture of durene and isodurene by stripping crystallization
1Department of Chemical and Materials Engineering, Chang Gung University, Taoyuan 333, Taiwan 2Department of Urology, Linkou Chang Gung Memorial Hospital, Taoyuan 333, Taiwan
shiau@mail.cgu.edu.tw
Korean Journal of Chemical Engineering, December 2021, 38(12), 2510-2518(9), 10.1007/s11814-021-0920-3
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Abstract
Stripping crystallization (SC) is introduced in this work to purify durene from the mixture consisting of isodurene and durene. SC is a new technology which combines melt crystallization and vaporization via a series of three-phase transformations at low pressures during the cooling process. The three-phase transformation conditions for a liquid mixture determined by the thermodynamic calculations were adopted to direct the batch SC experiments. A model based on the mass and energy balances was proposed to determine the variation of the amount of remaining liquid, crystallized durene product and produced vapor during SC. The experimental yield and purity of the final durene product obtained from the experiments were compared with those predicted by the model.
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Shiau LD, Yu CC, Sep. Purif. Technol., 66(2), 422 (2009)
Shiau LD, Liu KF, Hsu YC, Chem. Eng. Res. Des., 117, 301 (2017)
Shiau LD, Cryst. Growth Des., 20, 1328 (2020)
Kim KJ, Ulrich J, J. Colloid Interface Sci., 252(1), 161 (2002)
Ulrich J, Glade H, Melt crystallization: fundamentals, equipment and applications, Shaker Verlag, Germany (2003).
Li Q, Yi Z, Sun X, Su M, Korean J. Chem. Eng., 27(2), 619 (2010)
Jiang XB, Hou BH, He GH, Wang JK, Chem. Eng. Sci., 84, 120 (2012)
Beierling T, Osiander J, Sadowski G, Sep. Purif. Technol., 118, 13 (2013)
Micovic J, Beierling T, Lutze P, Sadowsk G, Gorak A, Chem. Eng. Process: Process Intensif., 67, 16 (2013)
Jiang XB, Li M, He GH, Wang JK, Ind. Eng. Chem. Res., 53(34), 13211 (2014)
Fukui K, Fujikawa T, Satone H, Yamamoto T, Maeda K, Kuramochi H, Chem. Eng. Sci., 143, 114 (2016)
Ahmad M, Ulrich J, Chem. Eng. Technol., 39(7), 1341 (2016)
Yazdanpanah N, Myerson A, Trout B, Ind. Eng. Chem. Res., 55(17), 5019 (2016)
Ioannou IS, Kontos SS, Koutsoukos PG, Paraskeva CA, Sep. Purif. Technol., 197, 8 (2018)
Jia S, Jing B, Gao Z, Gong J, Wang J, Rohani S, Sep. Purif. Technol., 259, 118140 (2021)
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Smith JM, Van Ness HC, Abbott MM, Introduction to chemical engineering thermodynamics, McGraw-Hill Book Co., Singapore (2001).
Sandler SI, Chemical, Biochemical, and Engineering Thermodynamics, John Wiley & Sons Inc., Asia (2006).