ISSN: 0256-1115 (print version) ISSN: 1975-7220 (electronic version)
Copyright © 2024 KICHE. All rights reserved

Articles & Issues

Language
English
Conflict of Interest
In relation to this article, we declare that there is no conflict of interest.
Publication history
Received February 14, 2022
Accepted August 10, 2022
articles This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
Copyright © KIChE. All rights reserved.

All issues

Dynamic simulation and control of a triple column process for dimethyl carbonate-methanol separation

Department of Mechanical Engineering, North University of China, No. 3 Xueyuan Road, Taiyuan, Shanxi, 030051, China 1Shanxi Province Key Laboratory of Higee-Oriented Chemical Engineering, North University of China, No. 3 Xueyuan Road, Taiyuan, Shanxi, 030051, China 2Low Carbon Energy Conversion Technology Research Center, Chinese Academy of Science, Shanghai, 201203, P. R. China, Chad
jwz0306@126.com
Korean Journal of Chemical Engineering, December 2022, 39(12), 3190-3203(14), 10.1007/s11814-022-1259-0
downloadDownload PDF

Abstract

Separation of dimethyl carbonate/methanol azeotropic mixture by using pressure-swing distillation process has been a hot-point in the study of the synthesis process of dimethyl carbonate by urea methanolysis method. This study updates the work of the writers (Ind.Eng.Chem.Res,2013,52,11463-11478), which explores the dynamic control structure of the three-column separation dimethyl carbonate (DMC)/methanol (MeOH) process from an actual pilot plant. At first, the conventional DMC/MeOH separation process in the pilot test of the DMC synthesis process through alcoholysis of urea was described in detail. Then an optimized control structure for the entire DMC/MeOH separation unit was obtained by implementing a general heuristic design procedure. An economic analysis was performed to evaluate the optimized process. Finally, three dynamic control schemes were proposed and evaluated with several large disturbances, an improved control scheme CS3, using the multiplier blocks “QR1/F1” and “RR1” in T1, “QR1/F1” and “R/F” in both T2 and T3, outperformed CS1 and CS2 by maintaining the product specification in each column.

References

Esan AO, Adeyemi AD, Ganesan S, J. Clean Prod., 257, 120561 (2020)
Kumar P, Srivastava VC, Stangar UL, Music B, Mishra IM, Meng Y, Catal. Rev.-Sci. Eng., 63, 363 (2021)
Labafzadeh SR, Helminen KJ, Kilpelainen I, King AWT, ChemSusChem, 8, 77 (2015)
Selva M, Perosa A, Rodriguez-Padron D, Luque R, ACS Sust. Chem. Eng., 7, 6471 (2019)
Tan KT, Lee KT, Mohamed AR, Fuel, 89, 3833 (2010)
Weidlich T, Chem. Listy., 109, 594 (2015)
Sun J, Yang B, Lin H, Chem. Eng. Technol., 27, 435 (2004)
Li CS, Zhang XP, Zhang SJ, Xu QQ, Chin. J. Process Eng., 453 (2003)
Wang SJ, Yu CC, Huang HP, Comput. Chem. Eng., 34, 361 (2010)
Zhang JL, Wang F, Peng WC, Xiao FK, Wei W, Sun YH, Petrochem. Eng., 39, 646 (2010)
Hsu KY, Hsiao YC, Chien IL, Ind. Eng. Chem. Res., 49, 735 (2010)
Wei HM, Wang F, Zhang JL, Liao B, Zhao N, Xiao FK, Wei W, Sun YH, Ind. Eng. Chem. Res., 52, 11463 (2013)
Zhao WB, Wang F, Peng WC, Zhao N, Li JP, Xiao FK, Wei W, Sun YH, Ind. Eng. Chem. Res., 47, 5913 (2008)
Wang DF, Zhang XL, Wei W, Sun YH, Chem. Eng. Technol., 35, 2183 (2012)
Wei HM, University of Chinese Academy of Sciences dissertation (2013).
Ma XB, Liu XG, Li ZH, Xu GH, Fluid Phase Equilib., 221, 51 (2004)
Luyben WL, Distillation design and control using AspenTM simulation, John Wiley & Sons: Inc: New York (2006).
Perkins JD, J. Chem. Technol. Biotechnol., 46, 249 (1989)
Turton R, Whiting WB, Shaeiwitz JA, Org. Proc. Res.-Dev., 3, 494 (1999)
Lin YJ, Wong D, Jang SS, Ou JJ, AIChE J., 58, 2697 (2012)
Luyben WL, AIChE J., 52, 2290 (2006)
Luyben WL, AIChE J., 52, 623 (2006)
Ward JD, Yu CC, Doherty MF, AIChE J., 53, 2885 (2007)
Grassi VG, Practical Distillation Control (1992).
Luyben WL, Ind. Eng. Chem. Res., 39, 973 (2000)
Luyben WL, AIChE J., 57, 655 (2011)

The Korean Institute of Chemical Engineers. F5, 119, Anam-ro, Seongbuk-gu, 233 Spring Street Seoul 02856, South Korea.
TEL. No. +82-2-458-3078FAX No. +82-507-804-0669E-mail : kiche@kiche.or.kr

Copyright (C) KICHE.all rights reserved.

- Korean Journal of Chemical Engineering 상단으로