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Received April 25, 2021
Accepted August 30, 2021
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Effect of nano MMT and mesoporous MCM-41 on corrosion resistance of poly (propylene carbonate) - based waterborne polyurethane
Department of Food and Drug Engineering, Shijiazhuang University of Applied Technology, No 12 Changxing Street, Qiaoxi District, Shijiazhuang Hebei 050081, China 1Shijiazhuang Flagship Coating Technology Co., Ltd., No 120 Huanghe Avenue, Gaoxin District, Shijiazhuang 050000, Hebei, China
shenao_07@163.com
Korean Journal of Chemical Engineering, April 2022, 39(4), 1036-1044(9), 10.1007/s11814-021-0944-8
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Abstract
Environmental friendly poly (propylene carbonate)-based waterborne polyurethane (PPC-based WPU) is prepared with PPC and isophorone diisocyanate (IPDI) as the soft segment and the hard segment, respectively. In this reaction system, 2,2-dimethylolbutyric acid (DMBA) is used as the hydrophilic donor and trimethylolpropane (TMP) as the crosslinking agent. The effect of co-doping of layered montmorillonite (MMT) and mesoporous material MCM- 41 on corrosion resistance of PPC-based WPU resin was studied. The properties of the samples were characterized with N2 physical adsorption, XRD, FT-IR, TG-DTA, DSC and water absorption testing. Potentiodynamic polarization curves, electrochemical impedance spectroscopy (EIS) and salt spray test were employed to investigate the corrosion performance of all the coatings. The results of XRD indicate that the MMT in the composite polyurethane resin is peeled off and MCM-41 maintains the hexagonal framework structure after grinding. Compared with the WPU coatings with MMT or MCM-41 single incorporation, those with MMT and MCM-41 co-incorporation show the best corrosion resistance, which is due to the different interface structure between filler and resin matrix.
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