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Received October 24, 2021
Accepted December 11, 2021
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Preparation of gold decorated MoS2/NiO nanocomposite in the production of a new electrochemical sensor for ascorbic acid detection
1Sakarya University, Biomedical, Magnetic and Semiconductor Materials Application and Research Center (BIMAS-RC), 54187 Sakarya, Turkey 2Sakarya University of Applied Sciences, Akyazı Vocational School of Health Services, 54400 Sakarya, Turkey 3Biomaterials, Energy, Photocatalysis, Enzyme Technology, Nano & Advanced Materials, Sakarya University, Environmental Applications and Sustainability Research & Development Group (BIOENAMS R & D Group), 54187 Sakarya, Turkey 4Science & Arts Faculty, Department of Chemistry, Sakarya University, 54187 Sakarya, Turkey
Korean Journal of Chemical Engineering, August 2022, 39(8), 2172-2181(10), 10.1007/s11814-021-1039-2
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Abstract
We investigated electrochemical sensing of ascorbic acid by Au-MoS2/NiO modified glassy carbon electrode. The MoS2, NiO, MoS2/NiO were prepared by hydrothermal , and Au-MoS2/NiO was prepared chemical reduction method. The characterization of Au-MoS2/NiO composite was carried out using X-ray diffraction, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and field emission scanning electron microscopy. The electrochemical characteristics of the Au-MoS2/NiO composite were examined by cyclic voltammetry and electrochemical impedance spectroscopy. Then, differential pulse voltammetry responses of Au-MoS2/NiO modified glassy carbon electrode were detected towards the ascorbic acid in phosphate buffer (0.1M, pH=7). The ascorbic acid sensor represented low detection limit of 0.13 μM with linear range of 2-50 μM, revealing that this sensor gave satisfactory responses. The practical feasibility of the obtained sensor was assessed for the detection of ascorbic acid in Vitamin C tablet. We believe that this study could help different studies for producing commercially ascorbic acid sensors.
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Yu H, Xu J, Liu Z, Li Y, Jin Z, J. Mater. Sci., 53, 15271 (2018)
Atacan K, J. Alloy. Compd., 791, 391 (2019)
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Nandapure BI, Kondawar SB, Chaudhari AM, Jamkar DV, Int. J. Curr. Eng. Sci. Res., 6, 438 (2019)
Gogoi P, Saikia BJ, Dolui SK, J. Appl. Polym. Sci., 132, 1 (2015)
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Zeng G, Li W, Ci S, Jia J, Wen Z, Sci. Rep., 6, 1 (2016)
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Gomes ES, Leite FRF, Ferraz BRL, Mourão HAJL, Malagutti AR, J. Pharm. Anal., 9, 347 (2019)
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Sha R, Bhattacharyya TK, Electrochim. Acta, 349, 136370 (2020)
Mahmoudi E, Hajian A, Rezaei M, Afkhami A, Amine A, Bagheri H, Microchem J., 145, 242 (2019)
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Li Y, Ye W, Cui Y, Li B, Yang Y, Qian G, J. Mol. Struct., 1209, 127986 (2020)
Erdurak-Kiliç CS, Uslu B, Dogan B, Ozgen U, Ozkan SA, Coskun M, J. Anal. Chem., 61, 1113 (2006)
Wei Y, Liu Y, Xu Z, Wang S, Chen B, Zhang D, Fang Y, Int. J. Anal. Chem., 2020, 1 (2020)
Bhajanthri NK, Arumugam VK, Chokkareddy R, Redhi GG, J. Mol. Liq., 222, 370 (2016)
Kaçar C, Erden PE, Anal. Bioanal. Chem., 412, 5315 (2020)
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Emran MY, Shenashen MA, Abdelwahab AA, Khalifa H, Mekawy M, Akhtar N, Abdelmottaleb M, El-Safty SA, J. Appl. Electrochem., 48, 529 (2018)
Xiao X, Zhang Z, Nan F, Zhao Y, Wang P, He F, Wang Y, J. Alloy. Compd., 852, 157045 (2021)
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Van der Horst C, Silwana B, Gil E, Iwuoha E, Somerset V, Electroanalysis, 32, 1 (2020)
Murugan N, Jerome R, Preethika M, Sundaramurthy A, Sundramoorthy AK, J. Mater. Sci. Technol., 72, 122 (2021)
