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Received November 15, 2021
Accepted December 28, 2021
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Differential pulse voltammetric sensor for tetracycline using manganese tungstate nanowafers and functionalized carbon nanofiber modified electrode
School of Chemical Engineering, Yeungnam University, Gyeongsan, Gyeongbuk 38541, Korea
Korean Journal of Chemical Engineering, August 2022, 39(8), 2192-2200(9), 10.1007/s11814-021-1055-2
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Abstract
A label-free approach was employed to selectively detect tetracycline using manganese tungstate (MnWO4) nanowafers and functionalized carbon nanofiber-modified glassy carbon electrode (GCE). MnWO4 nanowafers were synthesized hydrothermally and characterized along with functionalized carbon nanofibers (f-CNFs). Cyclic voltammetry and differential pulse voltammetry were employed to detect tetracycline, and the sensor exhibited linear ranges of detection of 1.75-109.25 μM and 109.25-409.25 μM, respectively. The limit of detection was found to be 0.24 μM (S/ N=3) with a sensitivity of 9.91 μA μM-1 cm-2. Interference studies were carried out with ciprofloxacin (Cip), penicillin (Pen), and amoxicillin (Amox). The modified electrode (MnWO4/f-CNF/GCE) was found to provide sensitive and selective detection of tetracycline in the presence of interfering agents.
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