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Received December 8, 2021
Accepted April 19, 2022
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Removal of heavy metal from aqueous medium using novel high-performance, antifouling, and antibacterial nanofiltration polyethersulfone membrane modified with green synthesized Ni-doped Al2O3
1Department of Chemical Engineering, Faculty of Engineering, Razi University, Kermanshah, Iran 2Chemical Engineering Advance Research Center, Razi University, Kermanshah, Iran 3Department of Applied Chemistry, Faculty of Chemistry, Razi University, Kermanshah, Iran 4Environmental Research Center, Department of Applied Chemistry, Razi University, Kermanshah, Iran
m.rahimi@razi.ac.ir
Korean Journal of Chemical Engineering, September 2022, 39(9), 2424-2443(20), 10.1007/s11814-022-1150-z
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Abstract
This study used green synthesized nickel-alumina nanoparticles (NANPs) to fabricate antifouling, antibacterial, and high-performance polyethersulfone (PES) nanofiltration membranes for heavy metal ion removal. Scrophularia striata extract was used to synthesize NANPs and to modify PES membranes. FT-IR, SEM, TEM, EDS, AFM, XRD, and zeta potential instrumental analyses were used to characterize NANPs and the membranes. The membrane porosity increased from 62.6% to 71.6-83.8%, and mean pore radius data exhibited a similar trend (from 4.47 to 7.54- 12.55 nm). The water contact angle of the membranes was reduced from 64.1o to 57.3o-47.1o owing to functionalities of NANPs, which improved membrane hydrophilicity and wettability. The prepared membrane water flux improved from 20.38 to 44.11-78.34 kg/m2h. The results reveal the enhancement antifouling resistance parameters for the blended membranes due to NANPs functionalities hydrogen bonding, membranes surface negative charge, and the smoother surface of the modified membranes, which AFM analysis proved. NANPs/PES membranes exhibited potent heavy metal ion removal and in the best case (0.5 wt% NANPs/PES membrane) the heavy metal rejection was Pb2+: 99.27%, Zn2+: 99.15%, Fe2+: 98.91%, and Cu2+: 98.58%. All the blended membranes showed effective antibacterial resistance against Escherichia coli (35.8-93.17%) and Staphylococcus aureus (37.3-94.25%) due to the presence of nickel and functionalities of NANPs.
Keywords
References
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Ghiggi FF, Pollo LD, Cardozo NSM, Tessaro IC, Eur. Polym. J., 92, 61 (2017)
Gholami S, Llacuna JL, Vatanpour V, Dehqan A, Paziresh S, Cortina JL, Chemosphere, 294, 133699 (2022)
Arefi-Oskoui S, Khataee A, Safarpour M, Vatanpour V, Sep. Purif. Technol., 238, 116495 (2020)
Vatanpour V, Paziresh S, Dehqan A, Asadzadeh-Khaneghah S, Habibi-Yangjeh A, Chemosphere, 279, 130616 (2021)
Li JH, Xu YY, Zhu LP, Wang JH, Du CH, J. Membr. Sci., 326, 659 (2009)
Balta S, Sotto A, Luis P, Benea L, der Bruggen BV, Kim J, J. Membr. Sci., 389, 155 (2012)
Mehrnia MR, Mojtahedi YM, Homayoonfal M, Desalination, 372, 75 (2015)
Lee KW, Seo BK, Nam ST, Han MJ, Desalination, 159, 289 (2003)
Humplik T, Lee J, O’Hern SC, Fellman BA, Baig MA, Hassan SF, Atieh MA, Rahman F, Laoui T, Karnik R, Wang EN, Nanotechnology, 22, 292001 (2011)
Koulivand H, Shahbazi A, Vatanpour V, Rahmandoost M, Mater. Sci. Eng. C-Biomimetic Supramol. Syst., 111, 110787 (2020)
Dervin S, Dionysiou DD, Pillai SC, Nanoscale, 8, 15115 (2016)
Vatanpour V, Esmaeili M, Farahani MHDA, J. Membr. Sci., 466, 70 (2014)
Peyravi M, Rahimpour A, Jahanshahi M, Javadi A, Shockravi A, Microporous Mesoporous Mater., 160, 114 (2012)
Sotto A, Boromand A, Balta S, Kim J, Der Bruggen BV, J. Mater. Chem., 21, 10311 (2011)
Kallem P, Bharath G, Rambabu K, Srinivasakannan C, Banat F, Chemosphere, 268, 129306 (2021)
Marjani A, Nakhjiri AT, Adimi M, Jirandehi HF, Shirazian S, Sci. Rep., 10, 2049 (2020)
Huang Z, Liu J, Liu Y, Xu Y, Li R, Hong H, Shen L, Lin H, Liao BQ, J. Membr. Sci., 623, 119080 (2021)
Bernstein R, Belfer S, Freger V, Environ. Sci. Technol., 45, 5973 (2011)
Shukla AK, Alam J, Alhoshan M, Dass LA, Ali FAA, Muthumareeswaran MR, Mishra U, Ansari MA, Environ. Sci. Water Res. Technol., 4, 438 (2018)
Tofighy MA, Mohammadi T, Chem. Eng. J., 388, 124192 (2020)
Xu S, Liu Y, Yu Y, Zhang X, Zhang J, Li Y, Sep. Purif. Technol., 235, 116185 (2020)
Porfírio DA, de Souza Borges Ferreira R, Malagutti AR, Valle EMA, Electrochim. Acta, 141, 33 (2014)
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