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Received September 12, 2021
Accepted November 22, 2021
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Powder X-ray diffraction analysis of Cu/Cu2O nanocomposites synthesized by colloidal solution method
Nguyen Hoang Lam
Nam Le
Eui Seon Kim
Mohaseen Salim Tamboli
Asiya Mohaseen Tamboli
Nguyen Tam Nguyen Truong†
Jae Hak Jung†
School of Chemical Engineering, Yeungnam University, 280 Daehak-ro, Gyeongsan 38541, Korea
Korean Journal of Chemical Engineering, September 2022, 39(9), 2505-2512(8), 10.1007/s11814-021-1024-9
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Abstract
Cu/Cu2O powder nanocomposites (PNCs) were successfully synthesized by colloidal solution method. To investigate the influence of oxidant agent concentration on the crystallite size and lattice constant of the PNCs, X-ray diffraction (XRD) was utilized to collect the database for crystal growth analysis. Due to the imperfect crystal growth, the Nelson-Riley function and the Williamson-Hall method were used to confirm the precise values of the PNCs. The Rietveld refinement method based on the XRD pattern was used. The XRD results show that the diffraction peaks were mainly assigned to the cubic structure, in good agreement with the ICDD standards. Furthermore, the change in oxidant agent concentration led to a very small change of microstrain in the peaks of Cu/Cu2O PNCs. Using these methods can aid in the precise study of the crystalline structure of the material, which can then be calculated to adjust the influencing conditions during the synthesis of the material.
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