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Received March 4, 2022
Accepted July 4, 2022
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Mesoporous ZnO nanoparticles using gelatin - Pluronic F127 as a double colloidal system for methylene blue photodegradation
Didik Prasetyoko1†
Novia Amalia Sholeha2
Riki Subagyo1
Maria Ulfa3
Hasliza Bahruji4
Holilah Holilah1
Mokhammad Fajar Pradipta5
Aishah Abdul Jalil6 7
1Department of Chemistry, Faculty of Science and Data Analytics, Institut Teknologi Sepuluh Nopember, Keputih, Sukolilo, Surabaya, 60111, Indonesia 2College of Vocational Studies, Bogor Agricultural University (IPB University), Jalan Kumbang No. 14, Bogor 16151, Indonesia 3Study Program of Chemistry Education, Faculty of Teacher Training and Education, Universitas Sebelas Maret,, Jl. Ir. Sutami 36A, 57126 Surakarta, Central Java, Indonesia 4Centre for Advanced Materials and Energy Sciences, Universiti Brunei Darussalam,, Jalan Tungku Link, Gadong BE1410, Brunei Darussalam 5Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Jl. Sekip Jogja, Central of Java, Indonesia 6Department of Chemical Engineering, Faculty of Chemical and Energy Engineering, Universiti Teknologi Malaysia, 81310 UTM, Skudai, Johor Bahru, Johor, Malaysia 7Centre of Hydrogen Energy, Institute of Future Energy, Universiti Teknologi Malaysia, Skudai, 81310 UTM, Skudai, Johor Bahru, Johor, Malaysia
didikp@chem.its.ac.id
Korean Journal of Chemical Engineering, January 2023, 40(1), 112-123(12), 10.1007/s11814-022-1224-y
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Abstract
ZnO nanoparticles with mesopores enhanced the photocatalytic degradation of dyes. The potential of gelatin-Pluronic F127 as a double colloidal system was investigated for constructing mesoporosity in ZnO nanoparticles. Amphoteric gelatin with hydrophobic and hydrophilic tails formed a stable colloid as the surface-active agent. The studies highlighted the effect of different zinc precursors (zinc acetate, zinc sulphate and zinc nitrate) on ZnO formation and methylene blue (MB) degradation activity. Porous ZnO nanoparticles with uniform hexagonal structures were formed when zinc acetate exhibited a higher photocatalytic activity. Unprecedented ZnSO4 resembling gunningite mineral was produced following high temperature calcination when using zinc sulfate as a precursor. The effect of temperature and concentration of MB solution indicated photodegradation reaction undergoes the first-order kinetic model. The mechanism of photocatalytic degradation of MB was determined using different types of scavenger agents, which indicated that hydroxyl radicals catalyzed the reaction.
Keywords
References
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Nandi P, Das D, Appl. Surf. Sci., 465, 546 (2019)
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Chen X, Wu Z, Liu D, Gao Z, Nanoscale Res. Lett., 12, 1 (2017)
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Mousavi SM, Mahjoub AR, Abazari R, J. Mol. Liq., 242, 512 (2017)
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Vinayagam R, Pai S, Murugesan G, Varadavenkatesan T, Selvaraj R, Appl. Nanosci. (2021)
Chan YY, Pang YL, Lim S, Chong WC, J. Environ. Chem. Eng., 9, 105417 (2021)
Goux A, Etienne M, Aubert E, Lecomte C, Ghanbaja J, Walcarius A, Chem. Mater., 21, 731 (2009)
Walcarius A, Sibottier E, Etienne M, Ghanbaja J, Nat. Mater., 6, 602 (2007)
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Ulfa M, Prasetyoko D, Mahadi AH, Bahruji H, Sci. Total Environ., 711, 135066 (2020)
Fang KM, Wang ZZ, Zhang M, Wang AJ, Meng ZY, Feng JJ, J. Colloid Interface Sci., 402, 68 (2013)
Tseng YH, Lin HY, Liu MH, Chen YF, Mou CY, J. Phys. Chem. C, 113, 18053 (2009)
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Lin Z, Du C, Yan B, Wang C, Yang G, Nat. Commun., 9, 1 (2018)
