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Received November 12, 2022
Revised March 3, 2023
Accepted March 19, 2023
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- The financial support of Istanbul Technical University under project ID MAB-2021-43188 (Dr. Olga Koba-Ucun) is acknowledged
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Reactive dye effluent treatment with peroxide-assisted ozonation: Effects of persulfate, peracetic acid and percarbonate
School of Civil Engineering, Department of Environmental Engineering, Istanbul Technical University, Ayazaga Campus, 34469 Maslak, Istanbul, Turkey
arslanid@itu.edu.tr
Korean Journal of Chemical Engineering, November 2023, 40(11), 2692-2700(9), 10.1007/s11814-023-1454-7
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Abstract
Simulated reactive dyebath effluent (pH11.0-11.5) bearing the commercially important textile azo dye
Reactive Red 21 (100 mg/L) can be successfully decolorized via ozone (feed rate=72 mg/min) and peroxide (=0.75-
6.00 mM)/ozone treatment processes. Persulfate (PS), peracetic acid (PAA) and percarbonate (PC) were selected as
alternative oxidants to the more conventional hydrogen peroxide. Color (peak absorbance) and total organic carbon
(TOC) removals increased with increasing PS concentration, but decreased when PC was introduced due to free radical scavenging effects of carbonate alkalinity. PAA improved color and TOC removal rates, but thereby also contributed to the TOC content of the dyebath effluent. PAA-assisted ozonation showed the highest performance in terms of
color removal at an optimum PAA concentration (=1.5 mM). According to the gas phase-and-dissolved ozone measurements, addition of the peroxides PS-PAA enhanced ozone decomposition and increased ozone absorption rates
whereas PC addition stabilized aqueous, molecular ozone. The originally non-toxic reactive dyebath effluent (10% relative inhibition) did not exhibit serious acute toxicity towards Vibrio fischeri photobacterium throughout ozonation and
ozone/PS treatment, whereas a slight increase was observed for ozone/PAA-ozone/PC that decreased with applied
ozone dose. The 7th-day-biochemical-oxygen-demand (BOD7; <10 mg/L) decreased with ozone dose speaking for less
biodegradable oxidation products
Keywords
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