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Language: English

Conflict of Interest: In relation to this article, we declare that there is no conflict of interest.

Publication history: Received June 16, 2022
Revised September 12, 2022
Accepted September 13, 2022

Acknowledgements: The authors gratefully acknowledge the Natural Science Foundation of Henan University of Technology (2020BS038) and Higher youth backbone teachers funded in colleges and universities of Henan province in 2019 (grant number 21220028).

This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

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One-step solvothermal synthesis of poly(arylene ether nitrile) decorated magnetic composite for methylene blue adsorption from aqueous solution

Xuefei Zhou¹ Wei Miao^1† Wenxi Cheng¹ Haowei Lin¹ Jinling Li¹ Hongjuan Zheng¹ Qiaohuan Cheng¹ Renjie Wang¹ Chenxue Yao¹ Xiaobo Liu^2†

¹School of Materials Science and Engineering, Henan University of Technology, Zhengzhou, 450001, China ²Research Branch of Advanced Functional Materials, School of Materials and Energy, University of Electronic Science and Technology of China, Chengdu, 610054, China

wei_miao@haut.edu.cn, liuxb@uestc.edu.cn

Korean Journal of Chemical Engineering, June 2023, 40(6), 1486-1496(11), 10.1007/s11814-022-1289-7

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Abstract

A series of poly(arylene ether nitrile) containing versatile carboxyl and sulfonic groups (CSPEN) were magnetically functionalized by ferroferric oxide (Fe3O4), and the obtained magnetic adsorbents (Fe3O4/CSPEN) were used to remove methylene blue (MB) dye from aqueous solution. The systematical characterizations that including scanning electron microscope (SEM), X-ray powder diffractometer (XRD), X-ray photoelectron spectroscopy (XPS), vibrating sample magnetometer (VSM), Fourier transform infrared (FTIR) certified that the Fe3O4/CSPEN possessed versatile functional groups and magnetic separation properties. The batch adsorption studies revealed that the Fe3O4/ CSPEN not only displayed high selective adsorption ability for cationic MB in the presence of anionic MO, but also exhibited a removal efficiency as high as 98.2%. Besides, the adsorption kinetics and isotherm matched well with pseudo-second-order model and Langmuir model, respectively, and the maximum adsorption capacity of Fe3O4/CSPEN for MB was 92.029 mg/g. The FTIR and Brunauer-Emmett-Teller (BET) analyses confirmed that the outstanding adsorption capacity of Fe3O4/CSPEN was attributed to their own microporous structure and the electrostatic interaction with MB. Therefore, the modified magnetic adsorbent can be used to selectively remove cationic dye from aqueous solution.

Keywords

Poly(Arylene Ether Nitrile) Fe3O4 Solvothermal Method Adsorption Methylene Blue

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