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- In relation to this article, we declare that there is no conflict of interest.
- Publication history
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Received September 13, 2022
Revised December 17, 2022
Accepted December 31, 2022
- Acknowledgements
- We acknowledge the financial support from the Ministry of Education, Culture, Research and Technology of the Republic of Indonesia under the World Class Professor award grant no. 3252/E4/ DT.04.03/2022.
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Photoelectrocatalysis performance of Se doped-TiO2/Ti nanotube arrays for visible-light-driven degradation of diazinon pesticide
Muhammad Nurdin1 2†
Abdul Haris Watoni1
Muhammad Natsir1
Sarifa Rahmatilah1
Maulidiyah Maulidiyah1
Dwiprayogo Wibowo2
La Ode Agus Salim3
La Ode Agus Salim4
Catherina Manukpadang Bijang5
Akrajas Ali Uma4
1Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Halu Oleo, Kendari 93232 - Southeast Sulawesi, Indonesia 2Department of Environmental Engineering, Universitas Muhammadiyah Kendari, Kendari 93127 - Southeast Sulawesi, Indonesia 3Department of Chemistry, Faculty of Science and Technology, Institut Sains Teknologi dan Kesehatan (ISTEK) ‘Aisyiyah Kendari, Kendari 93116 - Southeast Sulawesi, Indonesia 4Institute of Microengineering and Nanoelectronics, Universiti Kebangsaan Malaysia, UKM Bangi 43600 - Selangor, Malaysia 5Department of Chemistry, Faculty of Mathematics and Natural Sciences, Pattimura University, Ambon 97233 - Maluku, Indonesia
mnurdin06@yahoo.com
Korean Journal of Chemical Engineering, September 2023, 40(9), 2209-2218(10), 10.1007/s11814-023-1395-1
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Abstract
The modification of ternary metal oxide to improve the photoelectrocatalysis (PEC) properties of TiO2
photocatalyst is a hot issue in environmental and resource applications. Herein, we present a novel photoelectrocatalytst of Se doped-TiO2/Ti nanotube arrays (Se@TiO2/Ti-NTAs) for high-efficiency degradation of diazinon pesticide.
The Se@TiO2/Ti-NTAs were prepared to treat the TiO2-NTAs in Se-TiO2 sol-gel for 10 min, which was followed by calcination in air at 200 o
C for 1 h. Optical absorption spectroscopy of the Se@TiO2/Ti-NTAs indicated that there is a redshift in the optical energy gap to 2.95 eV if compared to the pristine TiO2/Ti NTAs, which suggests that the new photoelectrocatalyst is photoactive under visible light irradiation. We evaluated the photoactivity of the sample by using it as
the photoelectrocatalyst in the degradation of diazinon pesticides under the PEC process. The results showed that the
Se@TiO2/Ti-NTAs can degrade 95.62% for 1 h under visible light irradiation, which is equivalent to the degradation
rate constant of 0.0183 s1
. For comparison, the pristine TiO2/Ti NTAs only degrades the diazinon as high as 87.65%,
even then under UV light irradiation. Our result also indicated that the Se@TiO2/Ti-NTAs promote active photoelectron transfer and active radical formation, such as •OH and •O2
, for rapid diazinon pesticide degradation. The
Se@TiO2/Ti-NTAs photoelectrode should be a potential platform for environmental pollution treatment
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