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Received June 15, 2022
Revised January 27, 2023
Accepted February 27, 2023
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Low-temperature synthesis and characterization of porous chromium terephthalate MIL-101(Cr) and its photocatalytic degradation of phenanthrene
Usman Abubakar Adamu1 2
Noor Hana Hanif Abu Bakar1†
Zakariyya Uba Zango3
Nonni Soraya Sambudi4 5
Anwar Iqba1
Mohd Hazwan Hussin1
Tuan Sherwyn Hamidon1
1Nanoscience Research Laboratory, School of Chemical Sciences, Universiti Sains Malaysia, 11800 Penang, Malaysia 2Department of Chemistry, Faculty of Sciences, Gombe State University, P.M.B. 127, Gombe, Nigeria 3College of Natural and Applied Sciences, Al-Qalam University Katsina, 2137, Katsina State, Nigeria 4Chemical Engineering Department, Universiti Teknologi PETRONAS, Seri Iskandar, Perak, Malaysia 5Department of Chemical Engineering, Faculty of Technological Industry, Universitas Pertamina, Simprug, Jakarta 12220, Indonesia
Korean Journal of Chemical Engineering, September 2023, 40(9), 2239-2252(14), 10.1007/s11814-023-1408-0
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Abstract
Low-temperature hydrothermal technique was employed for the synthesis of highly porous and crystalline
MIL-101(Cr) metal-organic frameworks series. The resulting as-synthesized MOFs were characterized by Fourier transform infrared (FTIR) spectroscopy, powdered X-ray diffraction (XRD), scanning electron microscopy (SEM), nitrogen
adsorption-desorption analysis, thermogravimetric analysis (TGA), photoluminescence (PL) spectroscopy, and ultraviolet-visible (UV-vis) diffuse reflectance spectroscopy. The photocatalytic activity of the MOFs was evaluated for degradation of phenanthrene (PHE) under visible light irradiation. Among the MOFs, MIL-101@160 has the highest Brunner
Emmett-Teller (BET) specific surface area and corresponding pore volume of 2,592.2 m2
g
1
and 1.09 cm3
g
1
, respectively. Furthermore, it has shown higher photocatalytic degradation of the PHE than other samples with 98% degradation efficiency achieved within 150 minutes.
Keywords
References
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38. N. K. Gupta, J. Bae, S. Kim and K. S. Kim, RSC Adv., 11, 8951 (2002).
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44. L. Wang and L. Zan, Sci. Rep., 9, 1 (2019).
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47. A. S. Belousov and E. V. Suleimanov, Green Chem., 23, 6172 (2021).
48. Khodkar, S. M. Khezri, A. Pendashteh, S. Khoramnejadian and L.Mamani, Toxicol. Ind. Health, 34, 842 (2018).
49. X. Zhao, Z. Cai, T. Wang, S. E. O'Reilly, W. Liu and D. Zhao, Appl.Catal. B: Environ., 187, 134 (2016).
50. Z. Cai, X. Zhao, T. Wang, W. Liu and D. Zhao, ACS Sust. Chem.Eng., 5, 547 (2017).
51. H. Bai, J. Zhou, H. Zhang and G. Tang, Colloids Surf. B Biointerfaces, 150, 68 (2017).
52. J. Fu, G. Z. Kyzas, Z. Cai, E. A. Deliyanni, W. Liu and D. Zhao,Chem. Eng. J., 335, 290 (2018).
53. A. Singh, B. Ahmed, A. Singh and A. K. Ojha, Spectrochim. Acta -Part A Mol. Biomol. Spectrosc., 204, 603 (2018).
54. S. Xue, J. Sun, Y. Liu, Z. Zhang, Y. Lin and Q. Liu, J. Hazard. Mater.,361, 30 (2019).
55. Z. Zhao, A. A. Omer, Z. Qin, S. Osman, L. Xia and R. P. Singh,Environ. Sci. Pollut. Res., 27, 17530 (2019).
56. J. Haodong, W. Liu, F. Sun, T. Huang, L. Chen, Y. Liu, J. Qi, C. Xie and D. Zhao, Chem. Eng. J., 419, 129605 (2021)
