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Received December 7, 2016
Accepted January 31, 2017
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Evaluation of Various Synthesis Methods for Calcite-Precipitated Calcium Carbonate (PCC) Formation
Department of R&D Team, Hanil Cement Corporation, Hanil Cement Corporation, 302, Maepo-ri, Maepo-eup, Danyang, Chungbuk, 27003, Korea 1Mineral Processing Division, Korea Institute of Geoscience and Mineral Resources (KIGAM), 124, Gwahak-ro, Yuseong-gu, Daejeon, 34132, Korea
ahnjw@kigam.re.kr
Korean Chemical Engineering Research, June 2017, 55(3), 279-286(8), 10.9713/kcer.2017.55.3.279 Epub 2 June 2017
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Abstract
This review paper evaluates different kinds of synthesis methods for calcite precipitated calcium carbonates by using different materials. The various processing routes of calcite with different compositions are reported and the possible optimum conditions required to synthesize a desired particle sizes of calcite are predicted. This paper mainly focuses on that the calcite morphology and size of the particles by carbonation process using loop reactors. In this regard, we have investigated various parameters such as CO2 flow rate, Ca (OH 2 concentration, temperature, pH effect, reaction time and loop reactor mechanism with orifice diameter. The research results illustrate the formation of well-defined and pure calcite crystals with controlled crystal growth and particle size, without additives or organic solvents. The crystal growth and particle size can be controlled, and smaller sizes are obtained by decreasing the Ca (OH)2 concentration and increasing the CO2 flow rate at lower temperatures with suitable pH. The crystal structure of obtained calcite was characterized by using X-ray diffraction method and the morphology by scanning electron microscope (SEM). The result of x-ray diffraction recognized that the calcite phase of calcium carbonate was the dominating crystalline structure.
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Ahn JW, Park JK, Lee SB, Cho HC, Han C, Kim H, Geosystem. Eng., 6(4), 106 (2003)
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Montes-Hernandez G, Fernandez-Martinez A, Charlet L, Tisserand D, Renard F, J. Cryst. Growth, 310(11), 2946 (2008)
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Thriveni T, Um N, Nam SY, Ahn YJ, Han C, Ahn JW, J. Korean Ceram. Soc., 51(2), 107 (2014)
Ahn JW, Joo SM, Kim HS, Kim DH, Kim JP, Kim H, Mater. Sci. Forum, 439, 244 (2003)
Ryu M, Ahn JW, You K, Goto S, Kim H, J. Ceram. Soc. Jpn., 117(1), 106 (2009)
Morales JG, Burgues JT, Clemente RR, J. Cryst. Growth, 169(2), 331 (1996)
Spanos N, Koutsoukos PG, J. Cryst. Growth, 191, 783 (1998)
Han YS, Hadiko G, Fuji M, Takahashi M, J. Cryst. Growth, 289(1), 269 (2006)
Jones L, Atkins P, Chemistry, 4th ed., Freeman WH, company, New York, NY(2003).
Ryu MY, You KS, Ahn JW, Kim H, Resour. Process., 54, 14 (2007)
Nishida I, Ultrason. Sonochem., 11(6), 423 (2004)
Sonawane SH, Gumfekar SP, Kate KH, Meshram SP, Kunte KJ, Ramjee L, Mahajan C, Parande MG, Ashokkumar M, Intern. J. Chem. Engin., 2010, 1 (2010)
