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Received October 7, 2016
Accepted February 22, 2017
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This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
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Solid Phase Extraction of Celecoxib from Drug Matrix and Biological Fluids by Grafted Poly β-cyclodextrine/allyl Amine Magnetic Nano-particles
Department of Chemistry, Islamic Azad University, Central Tehran Branch, Tehran, Iran 1Department of Chemistry, Research and Science Branch, Islamic Azad University, Tehran, Iran 2Department of Chemistry, Varamin (Pishva) Branch, Islamic Azad University, Varamin, Iran
h.ahmadpanahi@iauctb.ac.ir
Korean Chemical Engineering Research, June 2017, 55(3), 287-295(9), 10.9713/kcer.2017.55.3.287 Epub 2 June 2017
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Abstract
Using nanotechnology, magnetic nanoparticles of iron oxide were produced via co precipitation method and followed modification with organic compounds. In the next step, functionalized monomer was provided via coupling β-cyclodextrine and allylamine onto modified magnetic nanoparticles. These nanoparticles were used to establish the adsorption rate of celecoxib. Magnetic nanoparticles are modified by (3 mercaptopropyl trimethoxysilane. Nano-adsorbent was characterized by analytical and spectroscopic methods, such as Fourier transform infrared spectroscopy, elemental analysis, thermo-gravimetric analysis, and transmission electron microscopy (TEM). Laboratory parameters, such as the kinetics of adsorption isotherms, pH, reaction temperature and capacity were optimized. Finally, by using this nanoadsorbent in the optimized condition, extraction of celecoxib from biological samples as urine, drug matrix and blood plasma was carried out by high performance liquid chromatography with sensitivity and high accuracy.
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Qi LF, Wu LX, Zheng S, Wang YL, Fu HL, Cui DX, Biomacromolecules, 13(9), 2723 (2012)
Ruan J, Wang K, Song H, Xu X, Ji J, Cui D, Nanoscale. Res. Lett., 6, 1 (2011)
Nezhati MN, Panahi HA, Moniri E, Kelahrodi SR, Assadian F, Karimi M, Korean J. Chem. Eng., 27(4), 1269 (2010)
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Cole AJ, David AE, Wang J, Galban CJ, Hill HL, Yang VC, Biomaterials, 32, 2183 (2011)
Gupta AK, Gupta M, Biomaterials, 26, 3995 (2005)
Gupta AK, Naregalkar RR, Vaidya VD, Gupta M, Nanomedicine, 2, 23 (2007)
Villanueva A, Canete M, Roca AG, Calero M, Veintemillas- Verdaguer S, Serna CJ, Nanotechnol., 20, 115103 (2009)
Ye Y, Sun Y, Zhao H, Lan H, Gao M, Song F, Lou C, Li H, Wang W, Int. J. Pharm., 458, 110 (2013)
Mandavian AR, Mirrahimi MAS, Chem. Eng. J., 159(1-3), 264 (2010)
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Hall KL, Eagleton LC, Acrivos A, Vermeulen T, Ind. Eng. Chem. Fundam., 5, 212 (1966)
Frendlich HM, J. Phys. Chem., 57, 385 (1906)
Temkin MI, Pyzhev V, Acta Physiochim., 12, 327 (1940)
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