Articles & Issues
- Language
- korean
- Conflict of Interest
- In relation to this article, we declare that there is no conflict of interest.
- Publication history
-
Received June 21, 2006
Accepted June 23, 2006
-
This is an Open-Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/bync/3.0) which permits
unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.
Copyright © KIChE. All rights reserved.
All issues
분무열분해법에 의한 형광체 입자의 제조
Preparation of Fluorescence Particles by Spray Pyrolysis
건국대학교 화학공학과, 143-701 서울시 광진구 화양동 1 1공주대학교 화학공학과, 314-701 충남 공주시 신관동 182 2한국과학기술원 생명화학공학과, 305-701 대전시 유성구 구성동 373-1
Department of Chemical Engineering, Konkuk University, 1, Hwayang-dong, Gwangjin-gu, Seoul 143-701, Korea 1Department of Chemical Engineering, Gongju National Univeristy, 182, Shingwan-dong, Gongju-si, Chungnam 314-701, Korea 2Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology, 373-1, Guseong-dong, Yuseong-gu, Daejeon 305-701, Korea
SeungBinPark@kaist.ac.kr
Korean Chemical Engineering Research, June 2006, 44(3), 235-242(8), NONE Epub 19 July 2006
Download PDF
Abstract
분무 열분해법이란 전구체를 용해시킨 용액을 수 마이크론에서 수십 마이크론 크기의 액적으로 분무한 후, 용매를 증발시키고 석출된 전구체를 열분해하여, 입자 및 필름을 제조하는 공정이다. 이 분무 열분해법의 핵심 요소는 전구체, 용매, 액적 제조 그리고 분해 반응기 등 4가지이다. 이 4가지 요소의 적절한 조합에 의해서 현존하는 거의 대부분의 입자와 필름을 제조할 수 있는 범용성이 높은 기술이다. 현재 기술 수준으로는 상업적인 성공을 거두기는 힘들지만 향후 다성분계의 입자나 필름, 혹은 고기능성 입자의 제조에 응용될 경우 매우 유용한 기술로 각광을 받을 전망이다. 본 총설에서는 이 분문 열분해법을 이용해서 만들어지는 입자 중에서 주로 형광체를 중심으로 지금까지 개발된 다양한 분무 열분해 공정 기술을 소개한다.
Spray pyrosysis is a process to prepare particles and films by evaporating and decomposing droplets of precursor solutions in the order of 1-10 micrometer in diameter. Key elements of the spray pyrolysis process include precursor, solvent, droplet generator, and reactor. Various combination of these 4 elements produces wide range of particles and films. In general. the current status of the spray pyrolysis technology is not quite promising for commercial success. However, this process will be feasible to produce multicomponent functional materials of controlled morphology. In this paper, current status of the spray pyrolysis technology is introduced with the emphasis of production of fluorescence particles.
Keywords
References
Darabont A, Names-Incze P, Kertesz K, Tapaszto L, Koos AA, Osvath Z, Sarkozi Z, Vertesy Z, Horvath ZE, Biro LP, J. Optoelectron. Adv. M., 7(2), 631 (2005)
Roh HS, Kim EJ, Kang HS, Kang YC, Park HD, Park SB, Jpn. J. Appl. Phys., 42(5A), 2741 (2003)
Patil PS, Mater. Chem. Phys., 59(3), 185 (1999)
Kang YC, Roh HS, Park SB, J. European Ceram. Soc., 22(9-10), 1661 (2002)
Shimomura Y, Kijima N, J. Electrochem. Soc., 151(4), H86 (2004)
Shimomura Y, Kijima N, Electrochem. Solid State Lett., 7(2), H1 (2004)
Shimomura Y, Kijima N, Electrochem. Solid State Lett., 7(5), H18 (2004)
Shimomura Y, Kijima N, J. Electrochem. Soc., 151(8), H192 (2004)
Kang YC, Roh HS, Park SB, Adv. Mater., 12(6), 451 (2000)
Kang YC, Park SB, Lenggoro IW, Okuyama K, J. Mater. Res., 14(6), 2611 (1999)
Kang YC, Roh HS, Park SB, J. Electrochem. Soc., 147(4), 1601 (2000)
Kang YC, Seo DJ, Park SB, Park HD, Jpn. J. Appl. Phys., 40(6A), 4083 (2001)
Lee JH, Kang YC, Park SB, Park HD, Jpn. J. Appl. Phys., 40(5A), 3222 (2001)
Kang YC, Park HD, Park SB, Jpn. J. Appl. Phys., 39(12B), 1305 (2000)
Kang YC, Chung YS, Park SB, J. Am. Ceram. Soc., 82(8), 2056 (1999)
Kang YC, Lenggoro IW, Okuyama K, Park SB, J. Electrochem. Soc., 146(3), 1227 (1999)
Kang YC, Lenggoro IW, Park SB, Okuyama K, J. Solid State Chem., 146(1), 168 (1999)
Cho SH, Yoo JS, Lee JD, Choi JS, Park SB, The 3rd International Conference on the Science and Technology of Display Phosphors, 307 (1997)
Hong GY, Kwon SH, Yoo JS, Summers CJ, The 5th International Conference on the Science and Technology of Display Phosphors, 187 (1999)
Park IW, Choi CK, Yoo JS, The 6th International Conference on the Science and Technology of Display Phosphors, 175 (2000)
Kang YC, Park HD, “Preparation Method of Red Phosphor Particles with Spherical Shape,” KR. Patent No. 2001-0015232 (2001)
Kang YC, Lee DY, Park HD, “Preparation Method of Blue and Green Emitting Aluminate Phosphor Particle,” KR. Patent No. 2001-0023819 (2001)
Roh HS, Kang YC, Park SB, J. Colloid Interface Sci., 228(2), 195 (2000)
Roh HS, Kim EJ, Kang HS, Kang YC, Park HD, Park SB, Jpn. J. Appl. Phys., 42(5A), 2741 (2003)
Patil PS, Mater. Chem. Phys., 59(3), 185 (1999)
Kang YC, Roh HS, Park SB, J. European Ceram. Soc., 22(9-10), 1661 (2002)
Shimomura Y, Kijima N, J. Electrochem. Soc., 151(4), H86 (2004)
Shimomura Y, Kijima N, Electrochem. Solid State Lett., 7(2), H1 (2004)
Shimomura Y, Kijima N, Electrochem. Solid State Lett., 7(5), H18 (2004)
Shimomura Y, Kijima N, J. Electrochem. Soc., 151(8), H192 (2004)
Kang YC, Roh HS, Park SB, Adv. Mater., 12(6), 451 (2000)
Kang YC, Park SB, Lenggoro IW, Okuyama K, J. Mater. Res., 14(6), 2611 (1999)
Kang YC, Roh HS, Park SB, J. Electrochem. Soc., 147(4), 1601 (2000)
Kang YC, Seo DJ, Park SB, Park HD, Jpn. J. Appl. Phys., 40(6A), 4083 (2001)
Lee JH, Kang YC, Park SB, Park HD, Jpn. J. Appl. Phys., 40(5A), 3222 (2001)
Kang YC, Park HD, Park SB, Jpn. J. Appl. Phys., 39(12B), 1305 (2000)
Kang YC, Chung YS, Park SB, J. Am. Ceram. Soc., 82(8), 2056 (1999)
Kang YC, Lenggoro IW, Okuyama K, Park SB, J. Electrochem. Soc., 146(3), 1227 (1999)
Kang YC, Lenggoro IW, Park SB, Okuyama K, J. Solid State Chem., 146(1), 168 (1999)
Cho SH, Yoo JS, Lee JD, Choi JS, Park SB, The 3rd International Conference on the Science and Technology of Display Phosphors, 307 (1997)
Hong GY, Kwon SH, Yoo JS, Summers CJ, The 5th International Conference on the Science and Technology of Display Phosphors, 187 (1999)
Park IW, Choi CK, Yoo JS, The 6th International Conference on the Science and Technology of Display Phosphors, 175 (2000)
Kang YC, Park HD, “Preparation Method of Red Phosphor Particles with Spherical Shape,” KR. Patent No. 2001-0015232 (2001)
Kang YC, Lee DY, Park HD, “Preparation Method of Blue and Green Emitting Aluminate Phosphor Particle,” KR. Patent No. 2001-0023819 (2001)
Roh HS, Kang YC, Park SB, J. Colloid Interface Sci., 228(2), 195 (2000)
